allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside
CAS No.:1363461-66-8
Molecular Formula:C₈₄H₉₃Cl₃N₂O₂₃
Molecular Weight:1605.02
Hs Code.:

allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside

Synonyms:allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside

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Chemical Property of allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside

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Technology Process of allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside

There total 2 articles about allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1351706-67-6
benzyl ((N-phenyl)trifluoroacetimidoyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosyl)onate

: 1363461-65-7
allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-3-O-benzyloxycarbonyl-2-deoxy-α-D-glucopyranoside

: 1363461-66-8
allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside

Guidance literature:: With t-butyldimethylsiyl triflate; In cyclopentyl methyl ether; at 0 ℃; for 0.333333h; optical yield given as %de; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201003581

Reference yield:

: 1351706-67-6
benzyl ((N-phenyl)trifluoroacetimidoyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosyl)onate

: 1363461-65-7
allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-3-O-benzyloxycarbonyl-2-deoxy-α-D-glucopyranoside

: allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside

: 1363461-66-8
allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside

Guidance literature:: With trifluorormethanesulfonic acid; In acetonitrile; at 0 ℃; for 0.25h; optical yield given as %de; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1055/s-0030-1260313

Reference yield:

: 1363461-66-8
allyl 2-allyloxycarbonylamino-4-O-benzyl-6-O-[6-O-[(benzyl-7,8-di-O-benzyl-3-deoxy-4,5-O-isopropylidene-α-D-manno-oct-2-ulopyranosid)onate]-4-O-benzyl-2-deoxy-3-O-(4-methoxyphenylmethyl)-2-(2,2,2-trichloroethoxycarbonylamino)-β-D-glucopyranosyl]-2-deoxy-α-D-glucopyranoside

: 1363462-08-1
C₈₁H₉₂N₂O₂₁

Guidance literature:: With copper(II) sulfate; acetic acid; zinc; In 1,4-dioxane; at 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/chem.201003581