4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol

Base Information

Chemical Name:4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol
CAS No.:169103-76-8
Molecular Formula:C₃₀H₃₈N₈O₉
Molecular Weight:654.68
Hs Code.:

4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol

Synonyms:4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol

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Chemical Property of 4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol

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Technology Process of 4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol

There total 1 articles about 4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: (3aR,4S,6S,7R,7aR)-6-Azido-7-hydroxy-4-methoxy-3-methyl-hexahydro-benzooxazol-2-one

: Acetic acid (3S,6R)-3-(2,4-dinitro-phenylamino)-6-{[methyl-((S)-1-phenyl-ethyl)-amino]-methyl}-tetrahydro-pyran-2-yl ester

: 169103-76-8
4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol

: 4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-β-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; for 1h; Ambient temperature;

Reference yield: 84.0%

: 169103-76-8
4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol

: 169103-92-8
4-azido-3-O-<2'-amino-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(methylamino)-L-chiro-inositol

Guidance literature:: With sodium hydroxide; In water; for 6h; Heating;

Reference yield:

: 169103-76-8
4-azido-1-N,2-O-carbonyl-1,4,5-trideoxy-3-O-<2'-(2,4-dinitrophenylamino)-6'-<(1S)-phenylethyl>-methylamino-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-6-O-methyl-1-(methylamino)-L-chiro-inositol

: 4-amino-3-O-<2'-amino-6'-(methylamino)-2',3',4',6'-tetradeoxy-α-L-erythro-hexopyranosyl>-1,4,5-trideoxy-6-O-methyl-1-(methylamino)-L-chiro-inositol tetrakishydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / 3percent methanolic NaOH / H₂O / 6 h / Heating

2: 77 percent / methanol; H₂O / 5 h / Ambient temperature

3: 83 percent / 2N HCl, H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr / Ambient temperature

With hydrogenchloride; sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; water;