Technology Process of C21H34O3
There total 10 articles about C21H34O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: NaI / acetone
2.1: K2CO3 / acetone / Heating
2.2: aq. KOH / ethanol
2.3: 73 percent / aq. HCl
3.1: 95 percent / PTSA / benzene / Heating
4.1: 98 percent / H2 / Pd/C / methanol
5.1: 77 percent / pyridine
6.1: 100 percent / NaI; NaHCO3 / acetone
7.1: t-BuLi / diethyl ether / -78 °C
7.2: 65 percent / diethyl ether
8.1: 100 percent / PTSA / ethanol; H2O
With
pyridine; hydrogen; tert.-butyl lithium; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; sodium iodide;
palladium on activated charcoal;
In
methanol; diethyl ether; ethanol; water; acetone; benzene;
DOI:10.1016/j.tetlet.2007.04.109
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: K2CO3 / acetone / Heating
1.2: aq. KOH / ethanol
1.3: 73 percent / aq. HCl
2.1: 95 percent / PTSA / benzene / Heating
3.1: 98 percent / H2 / Pd/C / methanol
4.1: 77 percent / pyridine
5.1: 100 percent / NaI; NaHCO3 / acetone
6.1: t-BuLi / diethyl ether / -78 °C
6.2: 65 percent / diethyl ether
7.1: 100 percent / PTSA / ethanol; H2O
With
pyridine; hydrogen; tert.-butyl lithium; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; sodium iodide;
palladium on activated charcoal;
In
methanol; diethyl ether; ethanol; water; acetone; benzene;
DOI:10.1016/j.tetlet.2007.04.109
