[3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol

Base Information

• Chemical Name: [3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol
• CAS No.: 101319-12-4
• Molecular Formula: C₂₃H₂₇NO₅
• Molecular Weight: 397.471

Synonyms:[3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol

Chemical Property of [3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol

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Technology Process of [3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol

There total 3 articles about [3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester (103536-28-3) → [3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol (101319-12-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1021/ja00894a022

Reference yield:

thebaine (115-37-7) → [3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol (101319-12-4)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene

2: nBu₂O / Heating

3: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; dibutyl ether; In diethyl ether; benzene;

DOI:10.1021/ja00894a022

Reference yield:

4,5α-epoxy-3,6-dimethoxy-17-methyl-6ξ,14ξ-etheno-morphin-7-ene-7,8-dicarboxylic acid dimethyl ester (18651-71-3) → [3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-o-phenylene]-bis-methanol (101319-12-4)

Guidance literature:

Multi-step reaction with 2 steps

1: nBu₂O / Heating

2: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; dibutyl ether; In diethyl ether;

DOI:10.1021/ja00894a022

upstream raw materials:

3-methoxy-6-(3-methoxy-8-methyl-7,8,9,10-tetrahydro-6H-2-oxa-8-aza-cycloocta[cd]inden-7-yl)-phthalic acid dimethyl ester

thebaine

4,5α-epoxy-3,6-dimethoxy-17-methyl-6ξ,14ξ-etheno-morphin-7-ene-7,8-dicarboxylic acid dimethyl ester

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