C₂₃H₂₂O₃

Base Information

Chemical Name:C₂₃H₂₂O₃
CAS No.:1315480-29-5
Molecular Formula:C₂₃H₂₂O₃
Molecular Weight:346.426
Hs Code.:

C<sub>23</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:C₂₃H₂₂O₃

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Chemical Property of C₂₃H₂₂O₃

Chemical Property:

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Technology Process of C₂₃H₂₂O₃

There total 1 articles about C₂₃H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29558-77-8
4-bromo-4'-hydroxybiphenyl

: 1315480-29-5
C₂₃H₂₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / butanone / 8 h / Reflux

2.1: n-butyllithium / tert-butyl methyl ether / 2 h / -20 °C / Inert atmosphere

2.2: -60 - 20 °C

2.3: 0.17 h / 20 °C

3.1: palladium diacetate; sodium carbonate; triphenylphosphine / propan-1-ol; toluene / 4 h / Reflux; Inert atmosphere

With n-butyllithium; palladium diacetate; sodium carbonate; potassium carbonate; triphenylphosphine; In propan-1-ol; tert-butyl methyl ether; toluene; butanone; 3.1: Suzuki reaction;
DOI:10.1016/j.ejmech.2012.01.054

Reference yield:

: 1315480-29-5
C₂₃H₂₂O₃

: 1334511-77-1
C₄₂H₅₄N₄O₉

Guidance literature:: Multi-step reaction with 2 steps

1.1: cetyltrimethylammonim bromide; potassium hydroxide / 5,5-dimethyl-1,3-cyclohexadiene / 3 h / Reflux

1.2: 0.5 h / pH 1 / Reflux

2.1: dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

2.2: 48 h / 20 °C

With dmap; cetyltrimethylammonim bromide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; potassium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
DOI:10.1016/j.ejmech.2012.01.054

Reference yield:

: 1315480-29-5
C₂₃H₂₂O₃

: 1369573-40-9
C₃₇H₄₆N₄O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: cetyltrimethylammonim bromide; potassium hydroxide / 5,5-dimethyl-1,3-cyclohexadiene / 3 h / Reflux

1.2: 0.5 h / pH 1 / Reflux

2.1: dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

2.2: 48 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C

With dmap; cetyltrimethylammonim bromide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; potassium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane;
DOI:10.1016/j.ejmech.2012.01.054