1-[2-methyl-5-(4-formylphenyl)-3-thienyl]-2-(2-methyl-3-benzothiophenyl) perfluorocyclopentene

Base Information

Chemical Name:1-[2-methyl-5-(4-formylphenyl)-3-thienyl]-2-(2-methyl-3-benzothiophenyl) perfluorocyclopentene
CAS No.:1344734-18-4
Molecular Formula:C₂₆H₁₆F₆OS₂
Molecular Weight:522.535
Hs Code.:

Synonyms:1-[2-methyl-5-(4-formylphenyl)-3-thienyl]-2-(2-methyl-3-benzothiophenyl) perfluorocyclopentene

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Chemical Property of 1-[2-methyl-5-(4-formylphenyl)-3-thienyl]-2-(2-methyl-3-benzothiophenyl) perfluorocyclopentene

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Technology Process of 1-[2-methyl-5-(4-formylphenyl)-3-thienyl]-2-(2-methyl-3-benzothiophenyl) perfluorocyclopentene

There total 16 articles about 1-[2-methyl-5-(4-formylphenyl)-3-thienyl]-2-(2-methyl-3-benzothiophenyl) perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₂₈H₂₀F₆O₂S₂

: 1344734-18-4
1-[2-methyl-5-(4-formylphenyl)-3-thienyl]-2-(2-methyl-3-benzothiophenyl) perfluorocyclopentene

Guidance literature:: With pyridine; toluene-4-sulfonic acid; In water; acetone; at 80 ℃;

Reference yield: 35.0%

: C₃₄H₃₈O₂S₂

: 1344734-18-4
1-[2-methyl-5-(4-formylphenyl)-3-thienyl]-2-(2-methyl-3-benzothiophenyl) perfluorocyclopentene

Guidance literature:: With pyridine; In water; acetone; for 24h; Reflux;
DOI:10.1016/j.dyepig.2014.03.023

Reference yield:

: 152431-65-7
3-(2-fluoro-3,3,4,4,5,5-hexafluorocyclopent-1-en-1-yl)-2-methylbenzo[b]thiophene

: 550348-57-7
3-bromo-5-(4-(1,3-dioxolan-2-yl)phenyl)-2-methylthiophene

: 1344734-18-4
1-[2-methyl-5-(4-formylphenyl)-3-thienyl]-2-(2-methyl-3-benzothiophenyl) perfluorocyclopentene

Guidance literature:: 3-bromo-5-(4-(1,3-dioxolan-2-yl)phenyl)-2-methylthiophene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

3-(2-fluoro-3,3,4,4,5,5-hexafluorocyclopent-1-en-1-yl)-2-methylbenzo[b]thiophene; In tetrahydrofuran; at -78 - 20 ℃; for 2h;

With pyridine; toluene-4-sulfonic acid; In acetone; at 60 ℃; for 18h;