28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-xylopyranoside

Base Information

• Chemical Name: 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-xylopyranoside
• CAS No.: 1609983-93-8
• Molecular Formula: C₉₈H₁₀₁NO₂₀
• Molecular Weight: 1612.87
• Mol file: 1609983-93-8.mol

Synonyms:28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-xylopyranoside

Chemical Property of 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-xylopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-xylopyranoside

There total 1 articles about 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate (1609983-87-0) + C28H22Cl3NO7 → 28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-xylopyranoside (1609983-93-8)

Guidance literature:

6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate; C₂₈H₂₂Cl₃NO₇; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - 20 ℃; for 1.5h; Molecular sieve;

DOI:10.1016/j.ejmech.2014.03.080

Reference yield:

28-O-6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate 3-O-2,3,4,6-tetra-O-benzoyl-β-D-xylopyranoside (1609983-93-8) → C91H95NO20

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; for 5h; under 760.051 Torr;

DOI:10.1016/j.ejmech.2014.03.080

upstream raw materials:

6-(2'-O-benzyl-phthalimido)-2,3,4-tri-O-benzoyl-6-deoxy-β-D-glucopyranosyl oleanate