C₂₀H₃₀O₅

Base Information

Chemical Name:C₂₀H₃₀O₅
CAS No.:943153-90-0
Molecular Formula:C₂₀H₃₀O₅
Molecular Weight:350.455
Hs Code.:

C<sub>20</sub>H<sub>30</sub>O<sub>5</sub>

Synonyms:C₂₀H₃₀O₅

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Chemical Property of C₂₀H₃₀O₅

Chemical Property:

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Technology Process of C₂₀H₃₀O₅

There total 13 articles about C₂₀H₃₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₄₆O₅Si

: 943153-90-0
C₂₀H₃₀O₅

Guidance literature:: Multi-step reaction with 8 steps

1: 10.92 g / PPTS / ethanol / 1 h / 60 °C

2: 93 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / 20 °C

3: 89 percent / t-BuOOH; (+)-DIPT / Ti(Oi-Pr)4 / CH₂Cl₂; toluene / 3 h / -24 °C

4: 93 percent / sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran / 2 h / 20 °C

5: 95 percent / CSA / CH₂Cl₂ / 1 h / 0 °C

6: 96 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C

7: sulfur trioxide; pyridine; triethylamine / CH₂Cl₂; dimethylsulfoxide / 0.5 h / 0 °C

8: 0.469 g / 18-crown-6; t-BuOK / tetrahydrofuran / 3 h / 0 °C

With pyridine; tert.-butylhydroperoxide; lithium aluminium tetrahydride; 18-crown-6 ether; L-(+)-diisopropyl tartrate; camphor-10-sulfonic acid; sulfur trioxide; potassium tert-butylate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; titanium(IV) isopropylate; In tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; toluene; 3: Sharpless asymmetric epoxidaion / 8: Wittig reaction;
DOI:10.1055/s-2007-965970

Reference yield:

: 943153-85-3
(5R,6S)-8-(tert-butyldiphenylsiloxy)-5-(methoxymethoxy)-6-methyloct-2-yn-1-ol

: 943153-90-0
C₂₀H₃₀O₅

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / lithium aluminum hydride / tetrahydrofuran / 3 h / 20 °C

2: 89 percent / t-BuOOH; (+)-DIPT / Ti(Oi-Pr)4 / CH₂Cl₂; toluene / 3 h / -24 °C

3: 93 percent / sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran / 2 h / 20 °C

4: 95 percent / CSA / CH₂Cl₂ / 1 h / 0 °C

5: 96 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C

6: sulfur trioxide; pyridine; triethylamine / CH₂Cl₂; dimethylsulfoxide / 0.5 h / 0 °C

7: 0.469 g / 18-crown-6; t-BuOK / tetrahydrofuran / 3 h / 0 °C

With pyridine; tert.-butylhydroperoxide; lithium aluminium tetrahydride; 18-crown-6 ether; L-(+)-diisopropyl tartrate; camphor-10-sulfonic acid; sulfur trioxide; potassium tert-butylate; tetrabutyl ammonium fluoride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; titanium(IV) isopropylate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 2: Sharpless asymmetric epoxidaion / 7: Wittig reaction;
DOI:10.1055/s-2007-965970

Reference yield:

: 943153-82-0
(E,5R,6S)-8-(tert-butyldiphenylsiloxy)-5-(methoxymethoxy)-6-methyloct-2-ene-1-ol

: 943153-90-0
C₂₀H₃₀O₅

Guidance literature:: Multi-step reaction with 6 steps

1: 89 percent / t-BuOOH; (+)-DIPT / Ti(Oi-Pr)4 / CH₂Cl₂; toluene / 3 h / -24 °C

2: 93 percent / sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran / 2 h / 20 °C

3: 95 percent / CSA / CH₂Cl₂ / 1 h / 0 °C

4: 96 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C

5: sulfur trioxide; pyridine; triethylamine / CH₂Cl₂; dimethylsulfoxide / 0.5 h / 0 °C

6: 0.469 g / 18-crown-6; t-BuOK / tetrahydrofuran / 3 h / 0 °C

With pyridine; tert.-butylhydroperoxide; 18-crown-6 ether; L-(+)-diisopropyl tartrate; camphor-10-sulfonic acid; sulfur trioxide; potassium tert-butylate; tetrabutyl ammonium fluoride; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; titanium(IV) isopropylate; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; 1: Sharpless asymmetric epoxidaion / 6: Wittig reaction;
DOI:10.1055/s-2007-965970