N-(benzyloxycarbonyl)-2-(aminomethylene)malonic acid benzyl tert-butyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-2-(aminomethylene)malonic acid benzyl tert-butyl ester
CAS No.:72594-87-7
Molecular Formula:C₂₃H₂₇NO₆
Molecular Weight:413.47
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-2-(aminomethylene)malonic acid benzyl tert-butyl ester

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Chemical Property of N-(benzyloxycarbonyl)-2-(aminomethylene)malonic acid benzyl tert-butyl ester

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Technology Process of N-(benzyloxycarbonyl)-2-(aminomethylene)malonic acid benzyl tert-butyl ester

There total 2 articles about N-(benzyloxycarbonyl)-2-(aminomethylene)malonic acid benzyl tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31037-42-0
hydroxymethyl carbamic acid benzyl ester

: 72594-87-7
N-(benzyloxycarbonyl)-2-(aminomethylene)malonic acid benzyl tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Et₃N / tetrahydrofuran / 4 h / Ambient temperature

2: 1.) NaH / 1.) THF, 15 min, 2.) THF, 2 h

With sodium hydride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jm00178a012