(S)-1-phenylethanaminium (S)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate

Base Information

Chemical Name:(S)-1-phenylethanaminium (S)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate
CAS No.:1352166-84-7
Molecular Formula:C₇H₈ClO₃P*C₈H₁₁N
Molecular Weight:327.748
Hs Code.:

Synonyms:(S)-1-phenylethanaminium (S)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate

Suppliers and Price of (S)-1-phenylethanaminium (S)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-phenylethanaminium (S)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate

Chemical Property:

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Technology Process of (S)-1-phenylethanaminium (S)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate

There total 2 articles about (S)-1-phenylethanaminium (S)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1352166-82-5
[α-hydroxy-(o-chlorophenyl)methyl]phosphinic acid

: (S)-1-phenylethanaminium (R)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate

: 1352166-84-7
(S)-1-phenylethanaminium (S)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate

Guidance literature:: In ethanol; for 5h; Reflux; Resolution of racemate;
DOI:10.1016/j.tetasy.2011.10.019

Reference yield:

: 89-98-5
2-chloro-benzaldehyde

: (S)-1-phenylethanaminium (R)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate

: 1352166-84-7
(S)-1-phenylethanaminium (S)-[α-hydroxy-(o-chlorophenyl)methyl]phosphinate

Guidance literature:: Multi-step reaction with 2 steps

1: hypophosphorous acid / ethanol / 48 h / Reflux

2: ethanol / 5 h / Reflux; Resolution of racemate

With hypophosphorous acid; In ethanol;
DOI:10.1016/j.tetasy.2011.10.019