tert-butyl (2-(2-(2-(2-nitrophenylsulfonamido)ethoxy)ethoxy)ethyl)carbamate

Base Information

Chemical Name:tert-butyl (2-(2-(2-(2-nitrophenylsulfonamido)ethoxy)ethoxy)ethyl)carbamate
CAS No.:943601-78-3
Molecular Formula:C₁₇H₂₇N₃O₈S
Molecular Weight:433.483
Hs Code.:

Synonyms:tert-butyl (2-(2-(2-(2-nitrophenylsulfonamido)ethoxy)ethoxy)ethyl)carbamate

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Chemical Property of tert-butyl (2-(2-(2-(2-nitrophenylsulfonamido)ethoxy)ethoxy)ethyl)carbamate

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Technology Process of tert-butyl (2-(2-(2-(2-nitrophenylsulfonamido)ethoxy)ethoxy)ethyl)carbamate

There total 9 articles about tert-butyl (2-(2-(2-(2-nitrophenylsulfonamido)ethoxy)ethoxy)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 943601-24-9
(2-[2-azidoethoxy]ethyl)-N-nosylethanamine

: 24424-99-5
di-tert-butyl dicarbonate

: 943601-78-3
tert-butyl (2-(2-(2-(2-nitrophenylsulfonamido)ethoxy)ethoxy)ethyl)carbamate

Guidance literature:: (2-[2-azidoethoxy]ethyl)-N-nosylethanamine; With triphenylphosphine; In tetrahydrofuran; water; at 20 ℃; for 1h;

di-tert-butyl dicarbonate; With sodium carbonate; In tetrahydrofuran; water; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/ol070376i

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 153086-78-3
tert-butyl {2-[2-(2-aminoethoxy)ethoxy]ethyl}carbamate

: 943601-78-3
tert-butyl (2-(2-(2-(2-nitrophenylsulfonamido)ethoxy)ethoxy)ethyl)carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: C₁₃H₂₀O₉S₂N₂

: 943601-78-3
tert-butyl (2-(2-(2-(2-nitrophenylsulfonamido)ethoxy)ethoxy)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3.15 g / sodium azide; tetra-n-butylammonium iodide / dimethylformamide / 1 h / 80 °C

2.1: triphenylphosphine / tetrahydrofuran; H₂O / 1 h / 20 °C

2.2: 53 percent / sodium carbonate / tetrahydrofuran; H₂O / 1 h / 20 °C

With sodium azide; tetra-(n-butyl)ammonium iodide; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/ol070376i