Technology Process of C12H11F3N2Se
There total 5 articles about C12H11F3N2Se which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide; triphenylphosphine;
In
tetrachloromethane; N,N-dimethyl-formamide;
at 90 ℃;
- Guidance literature:
-
C12H9ClF3NSe;
With
sodium azide; triphenylphosphine;
In
tetrachloromethane; N,N-dimethyl-formamide;
at 25 - 90 ℃;
With
water;
In
tetrachloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; pyridine / ethanol / 2 h / Inert atmosphere; Reflux
2.1: tetrahydrofuran / 12.83 h / 20 - 80 °C / Reflux
2.2: 0.33 h / 20 °C
3.1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 - -10 °C / Inert atmosphere
4.1: sodium azide; triphenylphosphine / N,N-dimethyl-formamide; tetrachloromethane / 90 °C
With
pyridine; hydrogenchloride; sodium azide; diisobutylaluminium hydride; triphenylphosphine;
In
tetrahydrofuran; tetrachloromethane; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;