Technology Process of 1,3-dimethyl-4-diphenylphosphorylimidazole-2-thione
There total 3 articles about 1,3-dimethyl-4-diphenylphosphorylimidazole-2-thione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
urea hydrogen peroxide adduct;
In
chloroform;
at 20 ℃;
for 24h;
DOI:10.1039/c2dt12483a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / -80 - -40 °C / Inert atmosphere
1.2: -80 - 20 °C / Inert atmosphere
2.1: urea hydrogen peroxide adduct / chloroform / 24 h / 20 °C
With
n-butyllithium; urea hydrogen peroxide adduct;
In
tetrahydrofuran; hexane; chloroform;
DOI:10.1039/c2dt12483a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: n-butyllithium / tetrahydrofuran / -80 °C / Schlenk technique; Inert atmosphere
2: urea hydrogen peroxide adduct / Schlenk technique; Inert atmosphere
With
n-butyllithium; urea hydrogen peroxide adduct;
In
tetrahydrofuran;
DOI:10.1039/c3dt51557e
