Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 6-methyl-, exo- (9CI)

Base Information

Chemical Name:Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 6-methyl-, exo- (9CI)
CAS No.:89521-22-2
Molecular Formula:C₉H₁₂O₂
Molecular Weight:152.193
Hs Code.:
Mol file:89521-22-2.mol

Synonyms:Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 6-methyl-, exo- (9CI)

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Chemical Property of Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 6-methyl-, exo- (9CI)

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Technology Process of Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 6-methyl-, exo- (9CI)

There total 2 articles about Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 6-methyl-, exo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-endo-Hydroxy-6-exo-methyl-8,9,10-trinorbornan-2-exo-carbonsaeure

: 89521-22-2
6-Methyl-8,9,10-trinorborn-5-en-2-exo-carbonsaeure

: 89521-21-1
6-Methyliden-8,9,10-trinorbornan-2-exo-carbonsaeure

Guidance literature:: With hydrogenchloride; potassium tert-butylate; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) 2.5 h; 2.) t-BuOH, 22 h, reflux;
DOI:10.1002/hlca.19830660834

Reference yield:

: 3212-14-4
2-methylbicyclo<2.2.1>hept-5-en-2endo-ol

: 89521-22-2
6-Methyl-8,9,10-trinorborn-5-en-2-exo-carbonsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg; 2.) 10percent NH₄Cl / 1.) Et₂O, 30 min; 2.) reflux

2: 1.) conc. HCl; 2.) t-BuOK / 1.) 2.5 h; 2.) t-BuOH, 22 h, reflux

With hydrogenchloride; potassium tert-butylate; ammonium chloride; magnesium;
DOI:10.1002/hlca.19830660834