N-tert-butyl ((4-methylbenzoato)(2-(pyridin-2-yl)phenyl)methyl)carbamate

Base Information

Chemical Name:N-tert-butyl ((4-methylbenzoato)(2-(pyridin-2-yl)phenyl)methyl)carbamate
CAS No.:1262642-59-0
Molecular Formula:C₂₅H₂₆N₂O₄
Molecular Weight:418.492
Hs Code.:

Synonyms:N-tert-butyl ((4-methylbenzoato)(2-(pyridin-2-yl)phenyl)methyl)carbamate

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Chemical Property of N-tert-butyl ((4-methylbenzoato)(2-(pyridin-2-yl)phenyl)methyl)carbamate

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Technology Process of N-tert-butyl ((4-methylbenzoato)(2-(pyridin-2-yl)phenyl)methyl)carbamate

There total 5 articles about N-tert-butyl ((4-methylbenzoato)(2-(pyridin-2-yl)phenyl)methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 877031-94-2
4-(t-butoxycarbonylimino-methyl)-benzoic acid methyl ester

: 1008-89-5
2-phenylpyridine

: 1262642-59-0
N-tert-butyl ((4-methylbenzoato)(2-(pyridin-2-yl)phenyl)methyl)carbamate

Guidance literature:: With silver hexafluoroantimonate; μ2-dichlorobis(chloro(cyclopentadienyl)rhodium); In dichloromethane; 2,4-dimethoxytoluene; at 75 ℃; for 20h;
DOI:10.1021/ja109562x

Reference yield:

: 4248-19-5
tert-butyl carbazate

: 1262642-59-0
N-tert-butyl ((4-methylbenzoato)(2-(pyridin-2-yl)phenyl)methyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / methanol; water

2: caesium carbonate / dichloromethane / 1 h / 20 °C

3: silver hexafluoroantimonate; μ2-dichlorobis(chloro(cyclopentadienyl)rhodium) / dichloromethane; 2,4-dimethoxytoluene / 20 h / 75 °C

With silver hexafluoroantimonate; formic acid; μ2-dichlorobis(chloro(cyclopentadienyl)rhodium); caesium carbonate; In methanol; dichloromethane; 2,4-dimethoxytoluene; water;
DOI:10.1021/ja109562x

Reference yield:

: 950522-67-5
N-tert-butyl (4-methoxycarbonylphenyl(phenylsulfonyl)methyl)carbamate

: 1262642-59-0
N-tert-butyl ((4-methylbenzoato)(2-(pyridin-2-yl)phenyl)methyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / dichloromethane / 1 h / 20 °C

2: silver hexafluoroantimonate; μ2-dichlorobis(chloro(cyclopentadienyl)rhodium) / dichloromethane; 2,4-dimethoxytoluene / 20 h / 75 °C

With silver hexafluoroantimonate; μ2-dichlorobis(chloro(cyclopentadienyl)rhodium); caesium carbonate; In dichloromethane; 2,4-dimethoxytoluene;
DOI:10.1021/ja109562x