phenyl-2,3,6-tri-O-acetyl-4-O-(2',3',4',6'-tetra-O-acetyl-β-d-galactopyranosyl)-1-selenenylsulfide-β-d-glucopyranoside

Base Information

Chemical Name:phenyl-2,3,6-tri-O-acetyl-4-O-(2',3',4',6'-tetra-O-acetyl-β-d-galactopyranosyl)-1-selenenylsulfide-β-d-glucopyranoside
CAS No.:1403574-84-4
Molecular Formula:C₃₂H₄₀O₁₇SSe
Molecular Weight:807.685
Hs Code.:

Synonyms:phenyl-2,3,6-tri-O-acetyl-4-O-(2',3',4',6'-tetra-O-acetyl-β-d-galactopyranosyl)-1-selenenylsulfide-β-d-glucopyranoside

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Chemical Property of phenyl-2,3,6-tri-O-acetyl-4-O-(2',3',4',6'-tetra-O-acetyl-β-d-galactopyranosyl)-1-selenenylsulfide-β-d-glucopyranoside

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Technology Process of phenyl-2,3,6-tri-O-acetyl-4-O-(2',3',4',6'-tetra-O-acetyl-β-d-galactopyranosyl)-1-selenenylsulfide-β-d-glucopyranoside

There total 2 articles about phenyl-2,3,6-tri-O-acetyl-4-O-(2',3',4',6'-tetra-O-acetyl-β-d-galactopyranosyl)-1-selenenylsulfide-β-d-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1666-13-3
diphenyl diselenide

: 4753-07-5
2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide

: 1403574-84-4
phenyl-2,3,6-tri-O-acetyl-4-O-(2',3',4',6'-tetra-O-acetyl-β-d-galactopyranosyl)-1-selenenylsulfide-β-d-glucopyranoside

Guidance literature:: 2,3,6,2',3',4',6'-hepta-O-acetyl-lactosyl bromide; With benzyltriethylammonium tetrathiomolybdate; In acetonitrile; at 25 ℃; for 2h;

diphenyl diselenide; In acetonitrile; at 25 ℃; for 4h;
DOI:10.1016/j.carres.2014.09.005

Reference yield:

: 1666-13-3
diphenyl diselenide

: hepta-O-acetyllactosyl iodide

: bis[2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1-4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranosyl]1,1'-disulfide

: 1403574-84-4
phenyl-2,3,6-tri-O-acetyl-4-O-(2',3',4',6'-tetra-O-acetyl-β-d-galactopyranosyl)-1-selenenylsulfide-β-d-glucopyranoside

Guidance literature:: hepta-O-acetyllactosyl iodide; With thiourea; In acetonitrile; at 60 ℃;

diphenyl diselenide; With triethylamine; In acetonitrile; at 20 ℃; for 0.25h;
DOI:10.1002/ejoc.201200299