1-(4,5-dimethoxy-2-nitrophenyl)-3-(4,5-methylenedioxy-2-nitrophenyl)-2-propen-1-one

Base Information

Chemical Name:1-(4,5-dimethoxy-2-nitrophenyl)-3-(4,5-methylenedioxy-2-nitrophenyl)-2-propen-1-one
CAS No.:76787-22-9
Molecular Formula:C₁₈H₁₄N₂O₉
Molecular Weight:402.317
Hs Code.:

Synonyms:1-(4,5-dimethoxy-2-nitrophenyl)-3-(4,5-methylenedioxy-2-nitrophenyl)-2-propen-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4,5-dimethoxy-2-nitrophenyl)-3-(4,5-methylenedioxy-2-nitrophenyl)-2-propen-1-one

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Technology Process of 1-(4,5-dimethoxy-2-nitrophenyl)-3-(4,5-methylenedioxy-2-nitrophenyl)-2-propen-1-one

There total 1 articles about 1-(4,5-dimethoxy-2-nitrophenyl)-3-(4,5-methylenedioxy-2-nitrophenyl)-2-propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 4101-32-0
4',5'-dimethoxy-2'-nitroacetophenone

: 712-97-0
6-nitro-1,3-benzodioxole-5-carbaldehyde

: 76787-22-9
1-(4,5-dimethoxy-2-nitrophenyl)-3-(4,5-methylenedioxy-2-nitrophenyl)-2-propen-1-one

Guidance literature:: With sodium hydroxide; In ethanol; 1. ice bath, 0.5h; 2. r.t., 4h;
DOI:10.1002/jhet.5570170726

Reference yield: 62.0%

: 76787-22-9
1-(4,5-dimethoxy-2-nitrophenyl)-3-(4,5-methylenedioxy-2-nitrophenyl)-2-propen-1-one

: 76787-30-9
2-(2-amino-4,5-dimethoxyphenyl)-7,8-dihydro<1,3>dioxolo<4,5-g>quinoline

Guidance literature:: With hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1002/jhet.5570170726

Reference yield:

: 76787-22-9
1-(4,5-dimethoxy-2-nitrophenyl)-3-(4,5-methylenedioxy-2-nitrophenyl)-2-propen-1-one

: 76787-31-0
2-(2-amino-4,5-dimethoxyphenyl)<1,3>dioxolo<4,5-g>quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / H₂ / 5percent palladium on carbon / dimethylformamide / Ambient temperature

2: 75 percent / 5percent palladium on carbon / various solvent(s) / 36 h / Heating

With hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570170726