triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside

Base Information

Chemical Name:triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside
CAS No.:1072450-39-5
Molecular Formula:C₇₆H₉₈O₁₇Si
Molecular Weight:1311.69
Hs Code.:

triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside

Synonyms:triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside

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Chemical Property of triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside

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Technology Process of triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside

There total 1 articles about triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1072450-38-4
triisopropylsilyl 4-O-acetyl-3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside

: 1072450-39-5
triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside

Guidance literature:: triisopropylsilyl 4-O-acetyl-3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside; With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 0.25h; Inert atmosphere;

With Glauber's salt; In hexane; dichloromethane; at -78 - 23 ℃; Inert atmosphere;
DOI:10.1002/anie.200801885

Reference yield: 89.0%

: 850004-29-4
5-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yloxy]-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-octanoic acid 1-sec-butyl-3-(tert-butyl-dimethyl-silanyloxy)-4-carboxy-butyl ester

: 1072450-39-5
triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside

: 1072450-40-8
C₁₂₉H₂₀₈O₂₇Si₆

Guidance literature:: 5-[3,4-bis-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yloxy]-3-(tert-butyl-dimethyl-silanyloxy)-6-methyl-octanoic acid 1-sec-butyl-3-(tert-butyl-dimethyl-silanyloxy)-4-carboxy-butyl ester; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In toluene; at 23 ℃; for 1.5h; Inert atmosphere;

triisopropylsilyl 3-O-benzyl-({[2,3,4-tri-O-benzyl-β-D-xylopyranosyl-(1->3)]-2,4-di-O-benzyl-β-D-xylopyranosyl-(1->4)}-2,3-di-O-isopropylidene-α-L-rhamnopyranosyl-(1->2))-β-D-fucopyranoside; With dmap; In toluene; at 23 ℃; for 4h; Inert atmosphere;
DOI:10.1002/anie.200801885