Technology Process of 5-Chlorosulfonyl-2-MethoxybenzoicAcid
There total 7 articles about 5-Chlorosulfonyl-2-MethoxybenzoicAcid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-methoxy-4-sulfobenzoic acid;
With
trichlorophosphate;
for 5h;
Reflux;
With
water;
DOI:10.1134/S1070428019080062
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water; iron; acetic acid / propan-1-ol / 2 h / Reflux
2: water; acetic acid; sodium nitrite / 0 - 90 °C
3: sodium hydroxide; water / 3 h / 20 - 70 °C
4: potassium permanganate; potassium carbonate; water / 80 °C
5: trichlorophosphate / 5 h / Reflux
With
potassium permanganate; water; iron; potassium carbonate; acetic acid; sodium hydroxide; sodium nitrite; trichlorophosphate;
In
propan-1-ol;
DOI:10.1134/S1070428019080062
- Guidance literature:
-
With
hydrogenchloride; sulfur dioxide; acetic acid; copper(l) chloride; sodium nitrite;
Yield given. Multistep reaction;
1.) H2O, -10 deg C, 5 min, 2.a) glac. acetic acid, 0-5 deg C, 2.b) 18 h, room temperature;
DOI:10.1002/ardp.19903230812
