C₅₀H₅₅Cl₆NO₁₇

Base Information

Chemical Name:C₅₀H₅₅Cl₆NO₁₇
CAS No.:186371-27-7
Molecular Formula:C₅₀H₅₅Cl₆NO₁₇
Molecular Weight:1154.7
Hs Code.:

C<sub>50</sub>H<sub>55</sub>Cl<sub>6</sub>NO<sub>17</sub>

Synonyms:C₅₀H₅₅Cl₆NO₁₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₀H₅₅Cl₆NO₁₇

Chemical Property:

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Technology Process of C₅₀H₅₅Cl₆NO₁₇

There total 3 articles about C₅₀H₅₅Cl₆NO₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 95603-44-4
7,10-di-(2,2,2-trichloroethyloxycarbonyl)-10-deacetylbaccatin III

: 186371-25-5
(S)-2-(((tert-butoxycarbonyl)amino)(phenyl)methyl)acrylic acid

: 186371-27-7
C₅₀H₅₅Cl₆NO₁₇

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In toluene; at 75 ℃; for 70h;
DOI:10.1039/P19960002869

Reference yield:

: 150884-50-7
benzaldehyde N-boc imine

: 186371-27-7
C₅₀H₅₅Cl₆NO₁₇

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) HMPA, DIBAL-H / 1.) hexane, toluene, 0 deg C, 1.5 h, 2.) toluene, -30 deg C, 16 h; -30 deg C to 0 deg C, 2 h

2: 70 percent / LiOH / H₂O; tetrahydrofuran / 48 h / 65 - 70 °C

3: 83 percent / DCC, DMAP / toluene / 70 h / 75 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; lithium hydroxide; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; In tetrahydrofuran; water; toluene;
DOI:10.1039/P19960002869

Reference yield:

: 186371-33-5
2-((S)-tert-Butoxycarbonylamino-phenyl-methyl)-acrylic acid (1R,2S)-2-phenyl-cyclohexyl ester

: 186371-27-7
C₅₀H₅₅Cl₆NO₁₇

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / LiOH / H₂O; tetrahydrofuran / 48 h / 65 - 70 °C

2: 83 percent / DCC, DMAP / toluene / 70 h / 75 °C

With dmap; lithium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; water; toluene;
DOI:10.1039/P19960002869