methyl N^δ-(tert-butoxycarbonyl)-N^α-[4-[3-(2,4-diamino-7H-pyrrolo[2,3-d]pyrimidin-5-yl)propyl]benzoyl]-L-ornithinate

Base Information

• Chemical Name: methyl N^δ-(tert-butoxycarbonyl)-N^α-[4-[3-(2,4-diamino-7H-pyrrolo[2,3-d]pyrimidin-5-yl)propyl]benzoyl]-L-ornithinate
• CAS No.: 303957-91-7
• Molecular Formula: C₂₇H₃₇N₇O₅
• Molecular Weight: 539.635

Synonyms:methyl N^δ-(tert-butoxycarbonyl)-N^α-[4-[3-(2,4-diamino-7H-pyrrolo[2,3-d]pyrimidin-5-yl)propyl]benzoyl]-L-ornithinate

Chemical Property of methyl N^δ-(tert-butoxycarbonyl)-N^α-[4-[3-(2,4-diamino-7H-pyrrolo[2,3-d]pyrimidin-5-yl)propyl]benzoyl]-L-ornithinate

Chemical Property:

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Technology Process of methyl N^δ-(tert-butoxycarbonyl)-N^α-[4-[3-(2,4-diamino-7H-pyrrolo[2,3-d]pyrimidin-5-yl)propyl]benzoyl]-L-ornithinate

There total 1 articles about methyl N^δ-(tert-butoxycarbonyl)-N^α-[4-[3-(2,4-diamino-7H-pyrrolo[2,3-d]pyrimidin-5-yl)propyl]benzoyl]-L-ornithinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

methyl Nδ-(tert-butoxycarbonyl)-L-ornithinate (51186-41-5) + 4-<2-(2,4-diamino-7H-pyrrolo<2,3-d>pyrimidin-5-yl)propyl>benzoic acid (134373-15-2) → methyl Nδ-(tert-butoxycarbonyl)-Nα-[4-[3-(2,4-diamino-7H-pyrrolo[2,3-d]pyrimidin-5-yl)propyl]benzoyl]-L-ornithinate (303957-91-7)

Guidance literature:

With triethylamine; diethyl dicarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1248/cpb.48.1270

Reference yield:

methyl Nδ-(tert-butoxycarbonyl)-Nα-[4-[3-(2,4-diamino-7H-pyrrolo[2,3-d]pyrimidin-5-yl)propyl]benzoyl]-L-ornithinate (303957-91-7) → 5-amino-2-{4-[3-(2,4-diamino-7H-pyrrolo[2,3-d]pyrimidin-5-yl)-propyl]-benzoylamino}-pentanoic acid methyl ester; hydrochloride

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 0.333333h;

DOI:10.1248/cpb.48.1270

upstream raw materials:

methyl N^δ-(tert-butoxycarbonyl)-L-ornithinate

4-<2-(2,4-diamino-7H-pyrrolo<2,3-d>pyrimidin-5-yl)propyl>benzoic acid

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