(2S,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine

Base Information

Chemical Name:(2S,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine
CAS No.:115245-58-4
Molecular Formula:C₂₂H₃₁NO₂
Molecular Weight:341.494
Hs Code.:

Synonyms:(2S,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine

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Technology Process of (2S,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine

There total 2 articles about (2S,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3806-59-5
1,3-cyclooctadiene

: 115245-58-4
(2S,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1) O₃, Me₂S; 2) 1N HCl / 1) MeOH; 2) acetone

2: diethyl ether / 12 h / Ambient temperature

With hydrogenchloride; dimethylsulfide; ozone; In diethyl ether;
DOI:10.1021/ja00223a053

Reference yield:

: 41980-05-6
oct-2t-enedial

: 532429-49-5
(4S,5R)-2-tert-Butyl-4-methyl-5-phenyl-oxazolidine

: 115303-94-1
(2R,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine

: 115245-58-4
(2S,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine

Guidance literature:: In diethyl ether; for 12h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1021/ja00223a053

Reference yield:

: 115245-58-4
(2S,4S,5R)-2-tert-Butyl-3-(1R,4aR,7aR)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-1-yl-4-methyl-5-phenyl-oxazolidine

: 115245-59-5,115303-96-3
[(3R,3aR,6aS)-3-((2S,4S,5R)-2-tert-Butyl-4-methyl-5-phenyl-oxazolidin-3-yl)-hexahydro-cyclopenta[c]furan-1-yl]-methanol

Guidance literature:: With pyridine; sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1) methanol;
DOI:10.1021/ja00223a053