all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-(8-aminooctyl)-1,3,5-triaminocyclohexane

Base Information

Chemical Name:all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-(8-aminooctyl)-1,3,5-triaminocyclohexane
CAS No.:688790-70-7
Molecular Formula:C₂₄H₄₈N₄O₄
Molecular Weight:456.67
Hs Code.:

Synonyms:all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-(8-aminooctyl)-1,3,5-triaminocyclohexane

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Chemical Property of all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-(8-aminooctyl)-1,3,5-triaminocyclohexane

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Technology Process of all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-(8-aminooctyl)-1,3,5-triaminocyclohexane

There total 6 articles about all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-(8-aminooctyl)-1,3,5-triaminocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 688790-67-2
all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-[8-N-(benzyloxycarbonyl)aminooctyl]-1,3,5-triaminocyclohexane

: 688790-70-7
all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-(8-aminooctyl)-1,3,5-triaminocyclohexane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 5h;
DOI:10.1021/ja039465q

Reference yield:

: 688790-64-9
all-cis-1,3-N,N'-(di-tert-butyloxycarbonyl)-1,3,5-triaminocyclohexane

: 688790-70-7
all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-(8-aminooctyl)-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 36 percent / diisopropylethylamine / acetonitrile / 192 h / pH 8 / Heating

2: 88 percent / H₂ / Pd/C / methanol / 5 h

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1021/ja039465q

Reference yield:

: 19008-71-0
8-aminooctan-1-ol

: 688790-70-7
all-cis-3,5-N,N-di-tert-butyloxycarbonyl-1-N-(8-aminooctyl)-1,3,5-triaminocyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1: 42 percent / triethylamine / methanol / 10 h / 20 °C

2: 88 percent / CBr₄; PPh₃ / CH₂Cl₂ / 0 - 20 °C

3: 36 percent / diisopropylethylamine / acetonitrile / 192 h / pH 8 / Heating

4: 88 percent / H₂ / Pd/C / methanol / 5 h

With carbon tetrabromide; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja039465q