(2E,2′E)-2,2′-[(2E,6E,8E,10E,14E)-2,6,11,15-tetramethyl-4,13-bis(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaene-1,16-diylidene]bis(1,1-dimethylhydrazine)

Base Information

Chemical Name:(2E,2′E)-2,2′-[(2E,6E,8E,10E,14E)-2,6,11,15-tetramethyl-4,13-bis(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaene-1,16-diylidene]bis(1,1-dimethylhydrazine)
CAS No.:1606991-77-8
Molecular Formula:C₃₆H₄₈N₄O₄S₂
Molecular Weight:664.934
Hs Code.:

Synonyms:(2E,2′E)-2,2′-[(2E,6E,8E,10E,14E)-2,6,11,15-tetramethyl-4,13-bis(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaene-1,16-diylidene]bis(1,1-dimethylhydrazine)

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Chemical Property of (2E,2′E)-2,2′-[(2E,6E,8E,10E,14E)-2,6,11,15-tetramethyl-4,13-bis(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaene-1,16-diylidene]bis(1,1-dimethylhydrazine)

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Technology Process of (2E,2′E)-2,2′-[(2E,6E,8E,10E,14E)-2,6,11,15-tetramethyl-4,13-bis(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaene-1,16-diylidene]bis(1,1-dimethylhydrazine)

There total 2 articles about (2E,2′E)-2,2′-[(2E,6E,8E,10E,14E)-2,6,11,15-tetramethyl-4,13-bis(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaene-1,16-diylidene]bis(1,1-dimethylhydrazine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1606991-76-7
(2E,2′E)-2,2′-{(2E,2′E,6E,6′E)-8,8′-sulfonylbis[2,6-dimethyl-4-(phenylsulfonyl)octa-2,6-dien-8-yl-1-ylidene]}bis(1,1-dimethylhydrazine)

: 1606991-77-8
(2E,2′E)-2,2′-[(2E,6E,8E,10E,14E)-2,6,11,15-tetramethyl-4,13-bis(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaene-1,16-diylidene]bis(1,1-dimethylhydrazine)

Guidance literature:: (2E,2′E)-2,2′-{(2E,2′E,6E,6′E)-8,8′-sulfonylbis[2,6-dimethyl-4-(phenylsulfonyl)octa-2,6-dien-8-yl-1-ylidene]}bis(1,1-dimethylhydrazine); With hexachloroethane; In dichloromethane; tert-butyl alcohol; at 20 ℃; for 0.166667h;

With potassium hydroxide; In dichloromethane; tert-butyl alcohol; at 20 ℃; for 2h;

Reference yield:

: 1606991-76-7
(2E,2′E)-2,2′-{(2E,2′E,6E,6′E)-8,8′-sulfonylbis[2,6-dimethyl-4-(phenylsulfonyl)octa-2,6-dien-8-yl-1-ylidene]}bis(1,1-dimethylhydrazine)

: 1606991-77-8
(2E,2′E)-2,2′-[(2E,6E,8E,10E,14E)-2,6,11,15-tetramethyl-4,13-bis(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaene-1,16-diylidene]bis(1,1-dimethylhydrazine)

: 1606991-85-8
(2E,2′E)-2,2′-[(2E,6E,8Z,10E,14E)-2,6,11,15-tetramethyl-4,13-bis(phenylsulfonyl)hexadeca-2,6,8,10,14-pentaene-1,16-diylidene]bis(1,1-dimethylhydrazine)

Guidance literature:: (2E,2′E)-2,2′-{(2E,2′E,6E,6′E)-8,8′-sulfonylbis[2,6-dimethyl-4-(phenylsulfonyl)octa-2,6-dien-8-yl-1-ylidene]}bis(1,1-dimethylhydrazine); With hexachloroethane; tert-butyl alcohol; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

With potassium hydroxide; In dichloromethane; at 20 ℃; for 2h; Overall yield = 56 %; Overall yield = 0.28 g; Inert atmosphere;
DOI:10.1021/jo500478u