(CF₃C₂CF₃)Co₂(CO)5(((C₆H₅)2P)2CH₂)

Base Information

Chemical Name:(CF₃C₂CF₃)Co₂(CO)5(((C₆H₅)2P)2CH₂)
CAS No.:108151-11-7
Molecular Formula:C₃₄H₂₂Co₂F₆O₅P₂
Molecular Weight:804.47
Hs Code.:

(CF<sub>3</sub>C<sub>2</sub>CF<sub>3</sub>)Co<sub>2</sub>(CO)5(((C<sub>6</sub>H<sub>5</sub>)2P)2CH<sub>2</sub>)

Synonyms:(CF₃C₂CF₃)Co₂(CO)5(((C₆H₅)2P)2CH₂)

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Chemical Property of (CF₃C₂CF₃)Co₂(CO)5(((C₆H₅)2P)2CH₂)

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Technology Process of (CF₃C₂CF₃)Co₂(CO)5(((C₆H₅)2P)2CH₂)

There total 3 articles about (CF₃C₂CF₃)Co₂(CO)5(((C₆H₅)2P)2CH₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 37685-63-5
{(carbonyl)3cobalt(μ-hexafluorobut-2-yne)cobalt(carbonyl)3}

: 2071-20-7
bis-diphenylphosphinomethane

: 108151-11-7
(CF₃C₂CF₃)Co₂(CO)5(((C₆H₅)2P)2CH₂)

Guidance literature:: With catalyst: benzophenone ketyl; In tetrahydrofuran; byproducts: CO; (Ar); at 288 K; catalytic amt. (< 0.1 mL) of benzophenone ketyl added to soln. of Co complex (0.27 mmol) and the ligand (0.32 mmol); immediate color change (from orane to red) observed; THF removed in vac.; residue sepd. on silica gel plates (hexane); only 1 band other than the parent complex developed; elution of this band with CH2Cl2 and crystn. from hexane gave the Co-phosphine complex; elem. anal.;

Reference yield: 85.0%

: 37685-63-5
{(carbonyl)3cobalt(μ-hexafluorobut-2-yne)cobalt(carbonyl)3}

: 2071-20-7
bis-diphenylphosphinomethane

: 108151-11-7
(CF₃C₂CF₃)Co₂(CO)5(((C₆H₅)2P)2CH₂)

: 108151-17-3
(CF₃C₂CF₃)Co₂(CO)4(((C₆H₅)2P)2CH₂)

: 84896-13-9,108151-17-3
{Co2(μ-CF3CCCF3)(CO)4(μ-dppm)}

Guidance literature:: In hexane; byproducts: CO; (Ar); soln. of equimolar amts. of Co complex and ligand refluxed for 5 h; react. mechanism discussed; solvent stripped in vac.; sepn. on silica gel plates (hexane/ether/CH2Cl2 10/1/1); 3 major bands developed, the 1. due to Co-Co-P complex, the 2. due to Co-Co-P2 complex, while the 3., on crystn. from hexane, gave P-Co-Co-P complex (elem. anal.);

Reference yield:

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 108151-11-7
(CF₃C₂CF₃)Co₂(CO)5(((C₆H₅)2P)2CH₂)

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent)

2: catalyst: benzophenone ketyl / tetrahydrofuran

With catalyst: benzophenone ketyl; In tetrahydrofuran;