2β-[3,4-(methylenedioxy)phenoxy]methyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane

Base Information

Chemical Name:2β-[3,4-(methylenedioxy)phenoxy]methyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane
CAS No.:440370-77-4
Molecular Formula:C₂₉H₃₁NO₅S
Molecular Weight:505.635
Hs Code.:

Synonyms:2β-[3,4-(methylenedioxy)phenoxy]methyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane

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Chemical Property of 2β-[3,4-(methylenedioxy)phenoxy]methyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane

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Technology Process of 2β-[3,4-(methylenedioxy)phenoxy]methyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane

There total 6 articles about 2β-[3,4-(methylenedioxy)phenoxy]methyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 533-31-3
Sesamol

: 440370-76-3
2β-trifluoromethanesulfonyloxymethyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane

: 2-methylene-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane

: 440370-77-4
2β-[3,4-(methylenedioxy)phenoxy]methyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane

Guidance literature:: Sesamol; With sodium; In tetrahydrofuran; at 20 ℃; for 0.5h;

2β-trifluoromethanesulfonyloxymethyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane; In tetrahydrofuran; dichloromethane; Further stages.;
DOI:10.1021/jo010973x

Reference yield:

: 130342-81-3
RTI-32

: 440370-77-4
2β-[3,4-(methylenedioxy)phenoxy]methyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-chloroethyl chloroformate / 1,2-dichloro-ethane / 24 h / Heating

1.2: 74 percent / 24 h / Heating

2.1: Et₃N / 0.25 h / -20 °C

2.2: 76 percent / 1 h / -20 °C

3.1: 83 percent / LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

4.1: collidine / CH₂Cl₂ / 1 h / -70 °C

5.1: Na / tetrahydrofuran / 0.5 h / 20 °C

5.2: 58 percent / tetrahydrofuran; CH₂Cl₂

With 2,3,5-trimethyl-pyridine; lithium aluminium tetrahydride; carbonochloridic acid 1-chloro-ethyl ester; sodium; triethylamine; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo010973x

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 440370-77-4
2β-[3,4-(methylenedioxy)phenoxy]methyl-3β-p-tolyl-N-(p-tolylsulfonamide)-tropane

Guidance literature:: Multi-step reaction with 4 steps

1.1: Et₃N / 0.25 h / -20 °C

1.2: 76 percent / 1 h / -20 °C

2.1: 83 percent / LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

3.1: collidine / CH₂Cl₂ / 1 h / -70 °C

4.1: Na / tetrahydrofuran / 0.5 h / 20 °C

4.2: 58 percent / tetrahydrofuran; CH₂Cl₂

With 2,3,5-trimethyl-pyridine; lithium aluminium tetrahydride; sodium; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo010973x