1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosylmethyl)-5-(p-toluenesulfonyl)-1H-tetrazole

Base Information

Chemical Name:1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosylmethyl)-5-(p-toluenesulfonyl)-1H-tetrazole
CAS No.:1075187-48-2
Molecular Formula:C₄₃H₄₄N₄O₇S
Molecular Weight:760.911
Hs Code.:

Synonyms:1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosylmethyl)-5-(p-toluenesulfonyl)-1H-tetrazole

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Chemical Property of 1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosylmethyl)-5-(p-toluenesulfonyl)-1H-tetrazole

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Technology Process of 1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosylmethyl)-5-(p-toluenesulfonyl)-1H-tetrazole

There total 1 articles about 1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosylmethyl)-5-(p-toluenesulfonyl)-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1075187-44-8
(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)methyl azide

: 19158-51-1
P-toluenesulfonyl cyanide

: 1075187-48-2
1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosylmethyl)-5-(p-toluenesulfonyl)-1H-tetrazole

Guidance literature:: at 100 ℃;
DOI:10.1021/jo801670k

Reference yield: 80.0%

: 1075187-48-2
1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosylmethyl)-5-(p-toluenesulfonyl)-1H-tetrazole

: 108149-63-9,108149-65-1
tert-butyl (4S)-4-(hydroxymethyl)-2,2-dimethyl-1,3-oxazolidine-3-carboxylate

: 1075187-67-5
(4R)-2,2-dimethyl-4-[1-(2',3',4',6'-tetra-O-benzyl-α-D-galactopyranosylmethyl)-1H-tetrazol-5-yloxymethyl]oxazolidine-3-carboxylic acid tert-butyl ester

Guidance literature:: tert-butyl (4S)-4-(hydroxymethyl)-2,2-dimethyl-1,3-oxazolidine-3-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.5h;

1-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosylmethyl)-5-(p-toluenesulfonyl)-1H-tetrazole; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 16h;
DOI:10.1021/jo801670k