2-{1,1-dimethyl-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-isoindole-1,3-dione

Base Information

Chemical Name:2-{1,1-dimethyl-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-isoindole-1,3-dione
CAS No.:808768-91-4
Molecular Formula:C₂₄H₂₈BNO₄
Molecular Weight:405.302
Hs Code.:

Synonyms:2-{1,1-dimethyl-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-isoindole-1,3-dione

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Chemical Property of 2-{1,1-dimethyl-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-isoindole-1,3-dione

Chemical Property:

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Technology Process of 2-{1,1-dimethyl-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-isoindole-1,3-dione

There total 3 articles about 2-{1,1-dimethyl-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-isoindole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-[2-(4-bromo-phenyl)-1,1-dimethyl-ethyl]-2-chloro-acetamide

: 808768-91-4
2-{1,1-dimethyl-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; thiourea / ethanol / 16 h / Heating / reflux

2: triethylamine / toluene / 16 h / 110 °C

3: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 16 h / 80 °C

With potassium acetate; acetic acid; triethylamine; thiourea; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ethanol; dimethyl sulfoxide; toluene;

Reference yield:

: 6186-22-7
4-bromophenyl acetone

: 808768-91-4
2-{1,1-dimethyl-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: methylmagnesium bromide / diethyl ether / 2 h / 0 - 20 °C

2.1: sulfuric acid / acetic acid / 4 h / 0 - 20 °C

2.2: 0 °C

3.1: acetic acid; thiourea / ethanol / 16 h / Heating / reflux

4.1: triethylamine / toluene / 16 h / 110 °C

5.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 16 h / 80 °C

With sulfuric acid; methylmagnesium bromide; potassium acetate; acetic acid; triethylamine; thiourea; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In diethyl ether; ethanol; acetic acid; dimethyl sulfoxide; toluene;

Reference yield:

: 57469-91-7
1-(4-bromophenyl)-2-methyl-propan-2-ol

: 808768-91-4
2-{1,1-dimethyl-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / acetic acid / 4 h / 0 - 20 °C

1.2: 0 °C

2.1: acetic acid; thiourea / ethanol / 16 h / Heating / reflux

3.1: triethylamine / toluene / 16 h / 110 °C

4.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 16 h / 80 °C

With sulfuric acid; potassium acetate; acetic acid; triethylamine; thiourea; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In ethanol; acetic acid; dimethyl sulfoxide; toluene;