1,2-bis(octyloxy)-4,5-dinitrobenzene

Base Information

• Chemical Name: 1,2-bis(octyloxy)-4,5-dinitrobenzene
• CAS No.: 156777-91-2
• Molecular Formula: C₂₂H₃₆N₂O₆
• Molecular Weight: 424.538
• Mol file: 156777-91-2.mol

Synonyms:1,2-bis(octyloxy)-4,5-dinitrobenzene

Chemical Property of 1,2-bis(octyloxy)-4,5-dinitrobenzene

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2-bis(octyloxy)-4,5-dinitrobenzene

There total 4 articles about 1,2-bis(octyloxy)-4,5-dinitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-bromo-octane (111-83-1) → 1,2-bis(octyloxy)-4,5-dinitrobenzene (156777-91-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / potassium carbonate / acetone / 48 h / Heating

2: 63 percent / nitric acid; acetic acid / CH₂Cl₂; H₂O / 0 - 20 °C

With nitric acid; potassium carbonate; acetic acid; In dichloromethane; water; acetone;

DOI:10.1021/jo035840l

Reference yield:

benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 1,2-bis(octyloxy)-4,5-dinitrobenzene (156777-91-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / potassium carbonate / acetone / 48 h / Heating

2: 63 percent / nitric acid; acetic acid / CH₂Cl₂; H₂O / 0 - 20 °C

With nitric acid; potassium carbonate; acetic acid; In dichloromethane; water; acetone;

DOI:10.1021/jo035840l

Reference yield:

1-bromo-octane (111-83-1) → 1,2-bis(octyloxy)-4,5-dinitrobenzene (156777-91-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / NaOH / H₂O / 48 h / Heating

2: 66 percent / 70percent HNO₃, conc. H₂SO₄ / acetic anhydride

With sodium hydroxide; sulfuric acid; nitric acid; In water; acetic anhydride;

upstream raw materials:

1-bromo-octane

benzene-1,2-diol

Downstream raw materials:

4,5-di(octyloxy)-2-nitroaniline

1,2-bis(octyloxy)-4,5-diaminobenzene

N,N'-bis<4,5-di(octyloxy)-2-nitrophenyl>oxamide

4,7-dibromo-5,6-bis(octyloxy)benzo-[c][1,2,5]-thiadiazole