C₅₈H₅₉NO₁₀Si

Base Information

Chemical Name:C₅₈H₅₉NO₁₀Si
CAS No.:1588523-50-5
Molecular Formula:C₅₈H₅₉NO₁₀Si
Molecular Weight:958.193
Hs Code.:

C<sub>58</sub>H<sub>59</sub>NO<sub>10</sub>Si

Synonyms:C₅₈H₅₉NO₁₀Si

Suppliers and Price of C₅₈H₅₉NO₁₀Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₈H₅₉NO₁₀Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₈H₅₉NO₁₀Si

There total 10 articles about C₅₈H₅₉NO₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1554004-75-9
benzyl 7-O-tetra-butyldiphenylsilyl-2,3,4-O-tri-benzyl-D-glycero-α-D-mannoheptopyranoside

: 62-23-7
4-nitro-benzoic acid

: 1588523-50-5
C₅₈H₅₉NO₁₀Si

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1016/j.bmc.2013.12.019

Reference yield:

: 530-26-7
D-Mannose

: 1588523-50-5
C₅₈H₅₉NO₁₀Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: acetyl chloride / 2 h / 50 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 6 h / 0 - 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 0.67 h / 20 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -40 °C / Inert atmosphere

6.2: 5 h / -40 - 20 °C

7.1: water; 4-methylmorpholine N-oxide; osmium(VIII) oxide / acetone / 4 h / 20 °C

8.1: 1H-imidazole / N,N-dimethyl-formamide / 6 h / 0 - 20 °C

9.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 5 h / 20 °C

With 1H-imidazole; osmium(VIII) oxide; n-butyllithium; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; water; sodium hydride; Dess-Martin periodane; 4-methylmorpholine N-oxide; acetyl chloride; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; mineral oil; 5.1: |Dess-Martin Oxidation / 6.1: |Wittig Olefination / 6.2: |Wittig Olefination / 9.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmc.2013.12.019

Reference yield:

: 102046-36-6
(2S,3S,4S,5S,6S)-3,4,5,6-tetrabenzyloxytetrahydropyran-2-carbaldehyde

: 1588523-50-5
C₅₈H₅₉NO₁₀Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -40 °C / Inert atmosphere

1.2: 5 h / -40 - 20 °C

2.1: water; 4-methylmorpholine N-oxide; osmium(VIII) oxide / acetone / 4 h / 20 °C

3.1: 1H-imidazole / N,N-dimethyl-formamide / 6 h / 0 - 20 °C

4.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 5 h / 20 °C

With 1H-imidazole; osmium(VIII) oxide; n-butyllithium; di-isopropyl azodicarboxylate; water; 4-methylmorpholine N-oxide; triphenylphosphine; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; acetone; 1.1: |Wittig Olefination / 1.2: |Wittig Olefination / 4.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmc.2013.12.019