1-[3-Eth-(E)-ylidene-2-methylene-cyclopentyloxymethyl]-4-methoxy-benzene

Base Information

• Chemical Name: 1-[3-Eth-(E)-ylidene-2-methylene-cyclopentyloxymethyl]-4-methoxy-benzene
• CAS No.: 131130-58-0
• Molecular Formula: C₁₆H₂₀O₂
• Molecular Weight: 244.334
• Mol file: 131130-58-0.mol

Synonyms:1-[3-Eth-(E)-ylidene-2-methylene-cyclopentyloxymethyl]-4-methoxy-benzene

Chemical Property of 1-[3-Eth-(E)-ylidene-2-methylene-cyclopentyloxymethyl]-4-methoxy-benzene

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[3-Eth-(E)-ylidene-2-methylene-cyclopentyloxymethyl]-4-methoxy-benzene

There total 2 articles about 1-[3-Eth-(E)-ylidene-2-methylene-cyclopentyloxymethyl]-4-methoxy-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

1-((E)-1-Ethynyl-hex-4-enyloxymethyl)-4-methoxy-benzene (131130-46-6) → 1-[3-Eth-(E)-ylidene-2-methylene-cyclopentyloxymethyl]-4-methoxy-benzene (131130-58-0) + C32H40O4

Guidance literature:

With palladium diacetate; tris(2,6-dimethoxyphenyl)phosphine; In benzene; for 0.67h; Ambient temperature;

DOI:10.1021/ja9624937

Reference yield:

1-((E)-1-Ethynyl-hex-4-enyloxymethyl)-4-methoxy-benzene (131130-46-6) → 1-Methoxy-4-(2-methylene-3-vinyl-cyclopentyloxymethyl)-benzene (185946-10-5) + 1-[3-Eth-(E)-ylidene-2-methylene-cyclopentyloxymethyl]-4-methoxy-benzene (131130-58-0)

Guidance literature:

With palladium diacetate; In benzene-d6; at 60 ℃; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

upstream raw materials:

1-((E)-1-Ethynyl-hex-4-enyloxymethyl)-4-methoxy-benzene