N¹-<3-<(Benzyloxycarbonyl)amino>propanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

Base Information

• Chemical Name: N¹-<3-<(Benzyloxycarbonyl)amino>propanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin
• CAS No.: 150671-86-6
• Molecular Formula: C₃₂H₄₂N₄O₇S₂
• Molecular Weight: 658.84

Synonyms:N¹-<3-<(Benzyloxycarbonyl)amino>propanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

Chemical Property of N¹-<3-<(Benzyloxycarbonyl)amino>propanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

Chemical Property:

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Technology Process of N¹-<3-<(Benzyloxycarbonyl)amino>propanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

There total 1 articles about N¹-<3-<(Benzyloxycarbonyl)amino>propanoyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → N1-<3-<(Benzyloxycarbonyl)amino>propanoyl>-N4,N8-bis(toluol-4-sulfonyl)spermidin (150671-86-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / NaOH / H₂O / 12 h / 0 °C

2: 1) 1,1'-carbonyldiimidazole / 1) THF, r.t., 2 h, 2) THF, r.t., 1 h

With sodium hydroxide; 1,1'-carbonyldiimidazole; In water;

DOI:10.1002/hlca.19930760304

Reference yield: 92.0%

N1-<3-<(Benzyloxycarbonyl)amino>propanoyl>-N4,N8-bis(toluol-4-sulfonyl)spermidin (150671-86-6) → N1-(β-Alanyl)-N4,N8-bis(toluol-4-sulfonyl)spermidin (150671-89-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 24h; under 760 Torr;

DOI:10.1002/hlca.19930760304

Reference yield:

N1-<3-<(Benzyloxycarbonyl)amino>propanoyl>-N4,N8-bis(toluol-4-sulfonyl)spermidin (150671-86-6) → (RS)-N1--β-alanyl>spermidin

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / H₂ / 10percent Pd/C / methanol / 24 h / 760 Torr

2: 1) 1,1'-carbonyldiimidazole / 1) THF, r.t., 2 h, 2) r.t., 1 h

3: 42 percent / Me₄NCl / ethanol / 5 °C / electrolysis (-2.4 V, SCE, cathode: Hg; anode: graphite)

With hydrogen; tetramethlyammonium chloride; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In methanol; ethanol;

DOI:10.1002/hlca.19930760304

upstream raw materials:

benzyl chloroformate

Downstream raw materials:

N¹-(β-Alanyl)-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

(RS)-N¹--β-alanyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

(RS)-N¹-alanyl>-β-alanyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

(RS)-N¹-alanyl>-β-alanyl>-N⁴,N⁸-bis(toluol-4-sulfonyl)spermidin

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