Benzoic acid benzoylamino-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl ester

Base Information

Chemical Name:Benzoic acid benzoylamino-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl ester
CAS No.:321970-55-2
Molecular Formula:C₂₆H₂₄N₂O₆
Molecular Weight:460.486
Hs Code.:

Synonyms:Benzoic acid benzoylamino-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl ester

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Chemical Property of Benzoic acid benzoylamino-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl ester

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Technology Process of Benzoic acid benzoylamino-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl ester

There total 2 articles about Benzoic acid benzoylamino-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: (S)-2-(2-Benzoylamino-2-bromo-acetylamino)-3-phenyl-propionic acid methyl ester

: 321970-55-2
Benzoic acid benzoylamino-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1021/ja0024800

Reference yield:

: 14281-55-1
PhCO-Gly-PheOMe

: 321970-55-2
Benzoic acid benzoylamino-((S)-1-methoxycarbonyl-2-phenyl-ethylcarbamoyl)-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-bromosuccinimide / CH₂Cl₂ / 3 h / Heating; irradiation

2: diisopropylethylamine / CH₂Cl₂ / 3 h / 0 °C

With N-Bromosuccinimide; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/ja0024800