C₃₉H₆₀O₂Si

Base Information

Chemical Name:C₃₉H₆₀O₂Si
CAS No.:1334336-42-3
Molecular Formula:C₃₉H₆₀O₂Si
Molecular Weight:588.99
Hs Code.:

C<sub>39</sub>H<sub>60</sub>O<sub>2</sub>Si

Synonyms:C₃₉H₆₀O₂Si

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Chemical Property of C₃₉H₆₀O₂Si

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Technology Process of C₃₉H₆₀O₂Si

There total 3 articles about C₃₉H₆₀O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 62938-08-3
3,5-di-tert-butylbenzyl bromide

: 57711-40-7
3-(O-tert-butyl(dimethyl)silyl)estrone

: 1334336-42-3
C₃₉H₆₀O₂Si

Guidance literature:: 3,5-di-tert-butylbenzyl bromide; With magnesium; In diethyl ether; at 20 ℃; for 2h; Inert atmosphere;

3-(O-tert-butyl(dimethyl)silyl)estrone; In tetrahydrofuran; diethyl ether; at 20 ℃; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether;
DOI:10.1016/j.ejmech.2011.06.027

Reference yield:

: 16225-26-6
3,5-di-tert-butylbenzoic acid

: 1334336-42-3
C₃₉H₆₀O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 1 h / 20 °C

3.1: magnesium / diethyl ether / 2 h / 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; carbon tetrabromide; magnesium; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; 3.1: Grignard reaction / 3.2: Grignard reaction;
DOI:10.1016/j.ejmech.2011.06.027

Reference yield:

: 77387-57-6
3,5-bis(1,1-dimethylethyl)benzenemethanol

: 1334336-42-3
C₃₉H₆₀O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 1 h / 20 °C

2.1: magnesium / diethyl ether / 2 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With carbon tetrabromide; magnesium; triphenylphosphine; In diethyl ether; dichloromethane; 2.1: Grignard reaction / 2.2: Grignard reaction;
DOI:10.1016/j.ejmech.2011.06.027