4(1H)-Pyrimidinethione, 6-amino-2-methyl- (9CI)

Base Information

• Chemical Name: 4(1H)-Pyrimidinethione, 6-amino-2-methyl- (9CI)
• CAS No.: 89280-06-8
• Molecular Formula: C₅H₇N₃S
• Molecular Weight: 141.197
• Hs Code.: 2933599090
• Mol file: 89280-06-8.mol

Synonyms:4(1H)-Pyrimidinethione,6-amino-2-methyl- (9CI); 4-Pyrimidinethiol, 6-amino-2-methyl- (7CI);6-Amino-2-methylpyrimidine-4-thiol

Chemical Property of 4(1H)-Pyrimidinethione, 6-amino-2-methyl- (9CI)

Chemical Property:

• PSA: 90.60000
• LogP: 1.23710

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4(1H)-Pyrimidinethione, 6-amino-2-methyl- (9CI)

There total 1 articles about 4(1H)-Pyrimidinethione, 6-amino-2-methyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 6-amino-2-methylpyrimidine-4-thiol (89280-06-8)

Guidance literature:

2-Methyl-6-amino-pyrimidinol-(4), 1. P2S5, Triaethylamin, Siedetemp., 2. W., Siedetemp.;

DOI:10.1248/cpb.11.912

Reference yield: 75.0%

6-amino-2-methylpyrimidine-4-thiol (89280-06-8) + 3-(chloromethyl)pyridine 1-oxide hydrochloride → 6-amino-2-methyl-4-(N-oxidopyridyl-3-methyl)thiopyrimidine (71208-66-7)

Guidance literature:

With sodium methylate; In N-methyl-acetamide;

Reference yield: 7.0%

2-(chloromethyl)-5-(3-chlorophenyl)-1,3-oxazole + 6-amino-2-methylpyrimidine-4-thiol (89280-06-8) → 6-([5-(3-chlorophenyl)-1,3-oxazol-2-yl]methylsulfanyl)-2-methylpyrimidin-4-amine

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 15h;

Downstream raw materials:

6-amino-2-methyl-4-(N-oxidopyridyl-3-methyl)thiopyrimidine

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