C₅₅H₉₈O₁₀Si₄

Base Information

Chemical Name:C₅₅H₉₈O₁₀Si₄
CAS No.:1338704-36-1
Molecular Formula:C₅₅H₉₈O₁₀Si₄
Molecular Weight:1031.72
Hs Code.:

C<sub>55</sub>H<sub>98</sub>O<sub>10</sub>Si<sub>4</sub>

Synonyms:C₅₅H₉₈O₁₀Si₄

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Chemical Property of C₅₅H₉₈O₁₀Si₄

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Technology Process of C₅₅H₉₈O₁₀Si₄

There total 23 articles about C₅₅H₉₈O₁₀Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1338704-15-6
C₄₃H₇₀O₁₀Si₂

: 69739-34-0
t-butyldimethylsiyl triflate

: 1338704-36-1
C₅₅H₉₈O₁₀Si₄

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1021/ol2024289

Reference yield:

: 1095272-57-3
C₂₃H₄₀O₇Si₂

: 1338704-36-1
C₅₅H₉₈O₁₀Si₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

1.2: 1.5 h / -78 °C

2.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.5 h / -78 °C

2.2: -78 - 0 °C

3.1: (1S)-10-camphorsulfonic acid / dichloromethane / 1 h / 25 °C

4.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C

With 2,6-dimethylpyridine; diethyl methoxy borane; phenylborondichloride; (1S)-10-camphorsulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; 1.1: Aldol addition / 1.2: Aldol addition;
DOI:10.1021/ol2024289

Reference yield:

: C₁₀H₁₈OS₂

: 1338704-36-1
C₅₅H₉₈O₁₀Si₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 0 - 25 °C

2.1: tetrahydrofuran; diethyl ether / -78 - 0 °C

3.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

3.2: 1 h / -78 °C

4.1: water; iodine; sodium hydrogencarbonate / acetonitrile / 0.08 h / 0 - 25 °C

5.1: sodium tetrahydroborate; diethyl methoxy borane / tetrahydrofuran; methanol / -78 - 0 °C

6.1: manganese(IV) oxide / dichloromethane / 3 h / 25 °C

7.1: 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; acetic acid / toluene / 72 h / 0 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 °C

9.1: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -78 °C

9.2: 1.5 h / -78 °C

10.1: diethyl methoxy borane / tetrahydrofuran; methanol / 0.5 h / -78 °C

10.2: -78 - 0 °C

11.1: (1S)-10-camphorsulfonic acid / dichloromethane / 1 h / 25 °C

12.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C

With 2,6-dimethylpyridine; manganese(IV) oxide; sodium tetrahydroborate; 1-(3,5-bis(trifluoromethyl)phenyl)-3-((1R,2R)-2-amino-1,2-diphenylethyl)thiourea; diethyl methoxy borane; phenylborondichloride; (1S)-10-camphorsulfonic acid; water; iodine; tert.-butyl lithium; sulfur trioxide pyridine complex; sodium hydrogencarbonate; acetic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane; toluene; acetonitrile; pentane; 9.1: Aldol addition / 9.2: Aldol addition;
DOI:10.1021/ol2024289