2-((1R,2R)-2-Hydroxymethyl-cyclohexyl)-2-methyl-thiopropionic acid O-ethyl ester

Base Information

Chemical Name:2-((1R,2R)-2-Hydroxymethyl-cyclohexyl)-2-methyl-thiopropionic acid O-ethyl ester
CAS No.:75967-87-2
Molecular Formula:C₁₃H₂₄O₂S
Molecular Weight:244.398
Hs Code.:

Synonyms:2-((1R,2R)-2-Hydroxymethyl-cyclohexyl)-2-methyl-thiopropionic acid O-ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((1R,2R)-2-Hydroxymethyl-cyclohexyl)-2-methyl-thiopropionic acid O-ethyl ester

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Technology Process of 2-((1R,2R)-2-Hydroxymethyl-cyclohexyl)-2-methyl-thiopropionic acid O-ethyl ester

There total 6 articles about 2-((1R,2R)-2-Hydroxymethyl-cyclohexyl)-2-methyl-thiopropionic acid O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₂₃O₂⁽¹⁺⁾*BF₄^(1-)

: 75967-87-2
2-((1R,2R)-2-Hydroxymethyl-cyclohexyl)-2-methyl-thiopropionic acid O-ethyl ester

Guidance literature:: With sodium hydrogensulfide; 18-crown-6 ether; In acetone; at -78 ℃;
DOI:10.1021/ja00545a039

Reference yield:

: C₁₃H₂₃O₂⁽¹⁺⁾*BF₄^(1-)

: 104395-05-3
(4aR,8aR)-4,4-Dimethyl-octahydro-isochromene-3-thione

: 75967-87-2
2-((1R,2R)-2-Hydroxymethyl-cyclohexyl)-2-methyl-thiopropionic acid O-ethyl ester

Guidance literature:: With sodium hydrogensulfide; 18-crown-6 ether; In acetone; at -78 ℃; for 5h;
DOI:10.1021/ja00281a040

Reference yield:

: (4aR,8aR)-3-Ethoxy-3-methoxy-4,4-dimethyl-octahydro-isochromene

: 75967-87-2
2-((1R,2R)-2-Hydroxymethyl-cyclohexyl)-2-methyl-thiopropionic acid O-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84.3 percent / BF₃*Et₂O

2: 18-crown-6, NaSH / acetone / 5 h / -78 °C

With sodium hydrogensulfide; 18-crown-6 ether; boron trifluoride diethyl etherate; In acetone;
DOI:10.1021/ja00281a040