methyl methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-α-L-idopyrnosiduronate-(1->4)-3,6-di-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:methyl methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-α-L-idopyrnosiduronate-(1->4)-3,6-di-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside
CAS No.:717902-54-0
Molecular Formula:C₃₈H₄₇NO₁₆
Molecular Weight:773.788
Hs Code.:

methyl methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-α-L-idopyrnosiduronate-(1->4)-3,6-di-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Synonyms:methyl methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-α-L-idopyrnosiduronate-(1->4)-3,6-di-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

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Chemical Property of methyl methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-α-L-idopyrnosiduronate-(1->4)-3,6-di-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

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Technology Process of methyl methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-α-L-idopyrnosiduronate-(1->4)-3,6-di-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

There total 2 articles about methyl methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-α-L-idopyrnosiduronate-(1->4)-3,6-di-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 615543-04-9
methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-L-idopyranosiduronate trichloroacetimidate

: 120001-96-9
methyl 2-benzyloxycarbonylamino-2-deoxy-3,6-di-O-acetyl-α-D-glucopyranoside

: 717902-54-0
methyl methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-α-L-idopyrnosiduronate-(1->4)-3,6-di-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -15 - 20 ℃; for 6h;
DOI:10.1021/jo035732z

Reference yield:

: 82877-93-8
methyl 3-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

: 717902-54-0
methyl methyl 2-O-acetyl-4-O-allyl-3-O-benzyl-α-L-idopyrnosiduronate-(1->4)-3,6-di-O-acetyl-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 2,4,6-collidine / -40 °C

2: 59 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 6 h / -15 - 20 °C

With 2,4,6-trimethyl-pyridine; trimethylsilyl trifluoromethanesulfonate; In dichloromethane;
DOI:10.1021/jo035732z