C₃₇H₆₁NO₁₁

Base Information

Chemical Name:C₃₇H₆₁NO₁₁
CAS No.:922166-96-9
Molecular Formula:C₃₇H₆₁NO₁₁
Molecular Weight:695.891
Hs Code.:

C<sub>37</sub>H<sub>61</sub>NO<sub>11</sub>

Synonyms:C₃₇H₆₁NO₁₁

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Chemical Property of C₃₇H₆₁NO₁₁

Chemical Property:

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Technology Process of C₃₇H₆₁NO₁₁

There total 25 articles about C₃₇H₆₁NO₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 922166-95-8
C₄₃H₇₅NO₁₁Si

: 922166-96-9
C₃₇H₆₁NO₁₁

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1021/ol062642i

Reference yield:

: 922166-82-3
N,N-diallyl-3-bromo-2,5-dimethoxyaniline

: 922166-96-9
C₃₇H₆₁NO₁₁

Guidance literature:: Multi-step reaction with 5 steps

1: 54 percent / n-BuLi / diethyl ether; hexane / 1.5 h / -78 °C

2: 100 percent / NaH / dimethylformamide / 0 - 20 °C

3: 97 percent / N,N-dimethylbarbituric acid; Pd(PPh₃)4 / CH₂Cl₂ / 2.5 h / Heating

4: 75 percent / Et₃N; N,N-dimethylaminopyridine / tetrahydrofuran / 6 h / Heating

5: TBAF / tetrahydrofuran / 24 h / 20 °C

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 1,3-dimethylbarbituric acid; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol062642i

Reference yield:

: tert-butyl-(4-methoxy-2-methyl-but-3-enyloxy)-diphenyl-silane

: 922166-96-9
C₃₇H₆₁NO₁₁

Guidance literature:: Multi-step reaction with 20 steps

1.1: 4.37 mg / aq. HCl / tetrahydrofuran; CH₂Cl₂ / 3 h / 20 °C

2.1: 96 percent / (S,S)-chiral titanium complex / diethyl ether; tetrahydrofuran / 5 h / -78 °C

3.1: 97 percent / KH / tetrahydrofuran / 0 - 20 °C

4.1: 98 percent / [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh; N-allyl-N-tritylamine; diisopropylethylamine / toluene / 3.5 h / Heating

5.1: OsO₄; H₂O; N-methylmorpholine N-oxide / acetone / 16 h / 20 °C

6.1: aq. NaIO₄ / acetone / 2.5 h / 20 °C

7.1: 2.73 g / 4 Angstroem molecular sieves / toluene / 2.5 h / -78 - 0 °C

8.1: 92 percent / KH / tetrahydrofuran / 0 - 20 °C

9.1: OsO₄; H₂O; N-methylmorpholine N-oxide / acetone / 18 h / 20 °C

10.1: aq. NaIO₄ / acetone / 2.5 h / 20 °C

11.1: s-BuLi / tetrahydrofuran; cyclohexane / 4.5 h / -78 - -20 °C

11.2: 1.18 g / citric acid / tetrahydrofuran; cyclohexane; H₂O / pH 4 - 5

12.1: BF₃*Et₂O / tetrahydrofuran; cyclohexane / -78 - -5 °C

12.2: 1.49 g / ethanolamine / pentane / 2.5 h / 0 °C

13.1: 94 percent / 2,6-lutidine / CH₂Cl₂ / 10 h / -78 °C

14.1: 82 percent / NH₄F; MeOH / 9.5 h / Heating

15.1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 4 h

16.1: 54 percent / n-BuLi / diethyl ether; hexane / 1.5 h / -78 °C

17.1: 100 percent / NaH / dimethylformamide / 0 - 20 °C

18.1: 97 percent / N,N-dimethylbarbituric acid; Pd(PPh₃)4 / CH₂Cl₂ / 2.5 h / Heating

19.1: 75 percent / Et₃N; N,N-dimethylaminopyridine / tetrahydrofuran / 6 h / Heating

20.1: TBAF / tetrahydrofuran / 24 h / 20 °C

With 2,6-dimethylpyridine; hydrogenchloride; methanol; dmap; ammonium fluoride; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 1,3-dimethylbarbituric acid; (S,S)-chiral titanium; [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh; 4 A molecular sieve; boron trifluoride diethyl etherate; N-tritylprop-2-en-1-amine; tetrabutyl ammonium fluoride; water; sec.-butyllithium; potassium hydride; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; cyclohexane; N,N-dimethyl-formamide; acetone; toluene; 11.1: Corey-Schlessinger olefination / 15.1: Dess-Martin oxidation;
DOI:10.1021/ol062642i