[Fe(benzene-1,4-bis(3-pyridin-2-ylurea))(benzene-1,4-bis(3-pyridin-2-ylurea)(-H))(8-hydroxyquinoline)]NO₃

Base Information

• Chemical Name: [Fe(benzene-1,4-bis(3-pyridin-2-ylurea))(benzene-1,4-bis(3-pyridin-2-ylurea)(-H))(8-hydroxyquinoline)]NO₃
• CAS No.: 1441177-71-4
• Molecular Formula: C₄₅H₃₇FeN₁₃O₅*NO₃
• Molecular Weight: 957.725

Synonyms:[Fe(benzene-1,4-bis(3-pyridin-2-ylurea))(benzene-1,4-bis(3-pyridin-2-ylurea)(-H))(8-hydroxyquinoline)]NO₃

Chemical Property of [Fe(benzene-1,4-bis(3-pyridin-2-ylurea))(benzene-1,4-bis(3-pyridin-2-ylurea)(-H))(8-hydroxyquinoline)]NO₃

Chemical Property:

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Technology Process of [Fe(benzene-1,4-bis(3-pyridin-2-ylurea))(benzene-1,4-bis(3-pyridin-2-ylurea)(-H))(8-hydroxyquinoline)]NO₃

There total 3 articles about [Fe(benzene-1,4-bis(3-pyridin-2-ylurea))(benzene-1,4-bis(3-pyridin-2-ylurea)(-H))(8-hydroxyquinoline)]NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.12%

Iron(III) nitrate nonahydrate + 8-quinolinol (148-24-3,24804-14-6) + benzene-1,4-bis(3-pyridin-2-ylurea) (1441177-78-1) → [Fe(benzene-1,4-bis(3-pyridin-2-ylurea))(benzene-1,4-bis(3-pyridin-2-ylurea)(-H))(8-hydroxyquinoline)]NO3 (1441177-71-4)

Guidance literature:

Iron(III) nitrate nonahydrate; benzene-1,4-bis(3-pyridin-2-ylurea); In ethanol; for 0.5h;

8-quinolinol; In ethanol; Reflux;

DOI:10.1016/j.saa.2013.03.016

Reference yield:

2-aminopyridine (504-29-0) → [Fe(benzene-1,4-bis(3-pyridin-2-ylurea))(benzene-1,4-bis(3-pyridin-2-ylurea)(-H))(8-hydroxyquinoline)]NO3 (1441177-71-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: piperidine / 6 h / Cooling with ice; Reflux

2.1: N,N-dimethyl-formamide / 4 h / Reflux

3.1: ethanol / 0.5 h

3.2: Reflux

With piperidine; In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.saa.2013.03.016

Reference yield:

ethyl 2-pyridinylcarbamate (5255-67-4) → [Fe(benzene-1,4-bis(3-pyridin-2-ylurea))(benzene-1,4-bis(3-pyridin-2-ylurea)(-H))(8-hydroxyquinoline)]NO3 (1441177-71-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 4 h / Reflux

2.1: ethanol / 0.5 h

2.2: Reflux

In ethanol; N,N-dimethyl-formamide;

DOI:10.1016/j.saa.2013.03.016

upstream raw materials:

ethyl 2-pyridinylcarbamate

8-quinolinol

benzene-1,4-bis(3-pyridin-2-ylurea)

2-aminopyridine

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