2-formylphenyl propanoate

Base Information

• Chemical Name: 2-formylphenyl propanoate
• CAS No.: 154366-28-6
• Molecular Formula: C₁₀H₁₀O₃
• Molecular Weight: 178.188
• Mol file: 154366-28-6.mol

Synonyms:2-formylphenyl propanoate

Chemical Property of 2-formylphenyl propanoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-formylphenyl propanoate

There total 3 articles about 2-formylphenyl propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

propionic acid 2-(hydroxyimino-methyl)-phenyl ester → 2-formylphenyl propanoate (154366-28-6)

Guidance literature:

With potassium permanganate; tungstate sulfuric acid; In dichloromethane; water; at 20 ℃; for 0.2h;

DOI:10.3390/11090720

Reference yield: 17.0%

→ o-propionyloxybenzoic acid (6328-44-5) + 2-formylphenyl propanoate (154366-28-6)

Guidance literature:

In dichloromethane; for 24h; Ambient temperature; Irradiation;

DOI:10.1016/0022-328X(93)83151-K

Reference yield: 17.0%

(C6H4OCHN)2C6H4CoCOC2H5 → 2-formylphenyl propanoate (154366-28-6)

Guidance literature:

In dichloromethane; Irradiation (UV/VIS); irradiation of Co-salophen-complex in dry CH2Cl2 under N2 at room temp. using a 300 W sunlamp for 24 h; monitoring by TLC, filtn. through a short pad of silica, concn. of filtrate in vacuo, column chromy. (silica, hexane/EtOAc);

DOI:10.1016/0022-328X(93)83151-K

Downstream raw materials:

3-methylcoumarine

2-methyl-benzyl alcohol

3-acetylcoumarin

ethyl coumarin-3-carboxylate