cis-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole

Base Information

• Chemical Name: cis-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole
• CAS No.: 1061352-24-6
• Molecular Formula: C₂₀H₂₀N₂
• Molecular Weight: 288.392

Synonyms:cis-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole

Chemical Property of cis-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole

Chemical Property:

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Technology Process of cis-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole

There total 2 articles about cis-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole (5094-12-2) + phenylacetylene (536-74-3) → cis-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole (1061352-24-6)

Guidance literature:

With tetrabutylammonium sulfate; potassium hydroxide; In water; dimethyl sulfoxide; at 20 - 80 ℃; Inert atmosphere;

Reference yield:

2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole (5094-12-2) + phenylacetylene (536-74-3) → cis-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole (1061352-24-6) + trans-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole (1061352-26-8)

Guidance literature:

With tetrabutylammonium sulfate; potassium hydroxide; In water; dimethyl sulfoxide; at 80 ℃; Inert atmosphere;

DOI:10.1016/j.bmcl.2009.11.037

Reference yield:

cis-2-methyl-5-(2-phenylethenyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole (1061352-24-6) → 2-methyl-5-(2-phenylethyl)-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole

Guidance literature:

With platinum(IV) oxide; hydrogen; for 12h; under 760.051 Torr;

DOI:10.1016/j.bmcl.2009.11.037

upstream raw materials:

2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole

phenylacetylene

Downstream raw materials:

cis-2-methyl-5-styryl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole hydrochloride

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