p-tolyl N-bis(dimethylamino)methylene-N'-(4-chlorophenyl)carbamimidothioate

Base Information

Chemical Name:p-tolyl N-bis(dimethylamino)methylene-N'-(4-chlorophenyl)carbamimidothioate
CAS No.:1564286-37-8
Molecular Formula:C₁₉H₂₃ClN₄S
Molecular Weight:374.937
Hs Code.:

Synonyms:p-tolyl N-bis(dimethylamino)methylene-N'-(4-chlorophenyl)carbamimidothioate

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Chemical Property of p-tolyl N-bis(dimethylamino)methylene-N'-(4-chlorophenyl)carbamimidothioate

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Technology Process of p-tolyl N-bis(dimethylamino)methylene-N'-(4-chlorophenyl)carbamimidothioate

There total 3 articles about p-tolyl N-bis(dimethylamino)methylene-N'-(4-chlorophenyl)carbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 624-31-7
4-tolyl iodide

: 1017963-91-5
C₁₂H₁₇ClN₄S

: 1564286-37-8
p-tolyl N-bis(dimethylamino)methylene-N'-(4-chlorophenyl)carbamimidothioate

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 10h; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.01.006

Reference yield:

: 80-70-6
N,N,N',N'-tetramethylguanidine

: 1564286-37-8
p-tolyl N-bis(dimethylamino)methylene-N'-(4-chlorophenyl)carbamimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 0.5 h

2: copper(l) iodide; 1,10-Phenanthroline; potassium carbonate / N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.01.006

Reference yield:

: 2131-55-7
4-Chlorophenyl isothiocyanate

: 1564286-37-8
p-tolyl N-bis(dimethylamino)methylene-N'-(4-chlorophenyl)carbamimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 0.5 h

2: copper(l) iodide; 1,10-Phenanthroline; potassium carbonate / N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.01.006