2-(4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzyloxy)-2-(4-(t-butoxydimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)tetrahydrofuran-3-ol

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Chemical Name:2-(4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzyloxy)-2-(4-(t-butoxydimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)tetrahydrofuran-3-ol
CAS No.:1246440-26-5
Molecular Formula:C₂₉H₄₂N₄O₁₀Si
Molecular Weight:634.759
Hs Code.:

Synonyms:2-(4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzyloxy)-2-(4-(t-butoxydimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)tetrahydrofuran-3-ol

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Chemical Property of 2-(4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzyloxy)-2-(4-(t-butoxydimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)tetrahydrofuran-3-ol

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Technology Process of 2-(4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzyloxy)-2-(4-(t-butoxydimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)tetrahydrofuran-3-ol

There total 1 articles about 2-(4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzyloxy)-2-(4-(t-butoxydimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)tetrahydrofuran-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1246440-25-4
4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzaldehyde

: 1246440-24-3
2-(4-(t-butyldimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)-2-methoxytetrahydrofuran-5-ol

: 1246440-26-5
2-(4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzyloxy)-2-(4-(t-butoxydimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)tetrahydrofuran-3-ol

Guidance literature:: 4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzaldehyde; 2-(4-(t-butyldimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)-2-methoxytetrahydrofuran-5-ol; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1039/c0cc01286f

Reference yield: 82.0%

: 1246440-26-5
2-(4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzyloxy)-2-(4-(t-butoxydimethylsilyloxy)-7-hydroxyhepta-1,5-diynyl)tetrahydrofuran-3-ol

: 1246440-27-6
2-(4-(2-(2-azidoethoxy)ethoxy)-5-methoxy-2-nitrobenzyloxy)-2-(7-bromo-4-(t-butoxydimethylsilyloxy)hepta-1,5-diynyl)tetrahydrofuran-3-ol

Guidance literature:: With 2,6-dimethylpyridine; carbon tetrabromide; triphenylphosphine; In acetonitrile; at 0 - 20 ℃;
DOI:10.1039/c0cc01286f