ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate

Base Information

Chemical Name:ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate
CAS No.:92592-16-0
Molecular Formula:C₂₀H₂₅N₃O₆S
Molecular Weight:435.501
Hs Code.:

Synonyms:ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate

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Chemical Property of ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate

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Technology Process of ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate

There total 6 articles about ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 60846-29-9
ethyl 2-amino-α-(N-(t-butoxycarbonyl)amino)-4-thiazoleacetate

: 501-53-1,94274-21-2
benzyl chloroformate

: 92592-16-0
ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate

: 92592-17-1
ethyl α-(3-benzyloxycarbonyl-2-benzyloxycarbonylimino-2,3-dihydrothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; for 16h;

Reference yield:

: 60845-81-0
ethyl 2-amino-α-(hydroxyimino)-4-thiazole acetate

: 92592-16-0
ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: H₂, HCl / 10percent Pd/C / ethanol

2: aq. K₂CO₃ / tetrahydrofuran / 24 h / Ambient temperature

3: aq. sodium bicarbonate / tetrahydrofuran; CH₂Cl₂ / Ambient temperature

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jm00092a006

Reference yield:

: 85208-11-3,92592-14-8
ethyl α-amino-α-(2-aminothiazol-4-yl)acetate dihydrochloride

: 92592-16-0
ethyl α-(2-benzyloxycarbonylaminothiazol-4-yl)-α-(t-butoxycarbonylamino)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. K₂CO₃ / tetrahydrofuran / 24 h / Ambient temperature

2: aq. sodium bicarbonate / tetrahydrofuran; CH₂Cl₂ / Ambient temperature

With sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00092a006