tert-butyl (2S)-2-{[3-(ethoxycarbonyl)phenyl](hydroxy)methyl}piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl (2S)-2-{[3-(ethoxycarbonyl)phenyl](hydroxy)methyl}piperidine-1-carboxylate
CAS No.:1094503-74-8
Molecular Formula:C₂₀H₂₉NO₅
Molecular Weight:363.454
Hs Code.:

Synonyms:tert-butyl (2S)-2-{[3-(ethoxycarbonyl)phenyl](hydroxy)methyl}piperidine-1-carboxylate

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Chemical Property of tert-butyl (2S)-2-{[3-(ethoxycarbonyl)phenyl](hydroxy)methyl}piperidine-1-carboxylate

Chemical Property:

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Technology Process of tert-butyl (2S)-2-{[3-(ethoxycarbonyl)phenyl](hydroxy)methyl}piperidine-1-carboxylate

There total 1 articles about tert-butyl (2S)-2-{[3-(ethoxycarbonyl)phenyl](hydroxy)methyl}piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58313-23-8
3-iodobenzoic acid methyl ester

: 150521-32-7,132910-78-2
(S)-1-N-Boc-piperidine-2-al

: 1094503-74-8
tert-butyl (2S)-2-{[3-(ethoxycarbonyl)phenyl](hydroxy)methyl}piperidine-1-carboxylate

Guidance literature:: 3-iodobenzoic acid methyl ester; With isopropylmagnesium bromide; In tetrahydrofuran; at -30 - -25 ℃; for 1.16667h; Inert atmosphere;

(S)-1-N-Boc-piperidine-2-al; In tetrahydrofuran; at -70 - -20 ℃;

With water; ammonium chloride; In tetrahydrofuran; at 0 ℃;

Reference yield:

: 129488-10-4
5-Amino-indazole-1-carboxylic acid tert-butyl ester

: 74124-79-1
di(succinimido) carbonate

: 1094503-74-8
tert-butyl (2S)-2-{[3-(ethoxycarbonyl)phenyl](hydroxy)methyl}piperidine-1-carboxylate

: 1094506-77-0
tert-butyl 5-[({[(2S)-1-(tert-butoxycarbonyl)piperid-2-yl][3(ethoxycarbonyl)phenyl]methoxy}carbonyl)amino]-1H-indazole-1-carboxylate

Guidance literature:: di(succinimido) carbonate; tert-butyl (2S)-2-{[3-(ethoxycarbonyl)phenyl](hydroxy)methyl}piperidine-1-carboxylate; With triethylamine; In acetonitrile; at 20 ℃; for 4h;

5-Amino-indazole-1-carboxylic acid tert-butyl ester; With triethylamine; In dichloromethane; at 20 ℃; for 16.1667h;