(1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester

Base Information

Chemical Name:(1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester
CAS No.:710965-73-4
Molecular Formula:C₃₀H₃₂O₆
Molecular Weight:488.58
Hs Code.:

Synonyms:(1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester

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Chemical Property of (1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester

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Technology Process of (1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester

There total 1 articles about (1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 80040-79-5
3,4,6-tri-O-benzyl-D-galactal

: 6832-16-2
methyl diazoacetate

: 710965-73-4
(1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester

Guidance literature:: dirhodium tetraacetate; In dichloromethane; at 23 ℃;
DOI:10.1021/ol070177z

Reference yield: 90.0%

: 710965-73-4
(1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester

: 935397-91-4
C₂₉H₃₂O₅

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 1h;
DOI:10.1021/ol070177z

Reference yield: 85.0%

: 15761-38-3
L-N-Boc-Ala

: 710965-73-4
(1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester

: C₃₈H₄₆INO₁₀

Guidance literature:: With N-iodo-succinimide; In dichloromethane; at 25 ℃; for 2h; diastereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.3987/COM-18-S(F)9