1-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁴-benzoyl cytosine

Base Information

• Chemical Name: 1-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁴-benzoyl cytosine
• CAS No.: 1020068-61-4
• Molecular Formula: C₃₈H₃₄FN₃O₇
• Molecular Weight: 663.702

Synonyms:1-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁴-benzoyl cytosine

Chemical Property of 1-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁴-benzoyl cytosine

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Technology Process of 1-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁴-benzoyl cytosine

There total 1 articles about 1-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁴-benzoyl cytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1-(2-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N4-benzoyl cytosine (1020068-59-0) + trityl chloride (76-83-5) → 1-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N4-benzoyl cytosine (1020068-61-4)

Guidance literature:

With pyridine; dmap; at 60 ℃; for 12h;

DOI:10.1016/j.ejmech.2007.04.001

Reference yield: 75.0%

1-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N4-benzoyl cytosine (1020068-61-4) → 1-(3-deoxy-3-fluoro-6-O-trityl-β-D-glycero-hex-2-enopyranosyl-4-ulose)-N4-benzoyl cytosine (1020068-64-7)

Guidance literature:

With dipyridinium dichromate; acetic anhydride; In dichloromethane; at 90 ℃; for 1.66667h;

DOI:10.1016/j.ejmech.2007.04.001

Reference yield: 55.0%

1-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N4-benzoyl cytosine (1020068-61-4) + phenylcarbonochloridothioate (1005-56-7) → 1-(2-O-acetyl-3-deoxy-3-fluoro-4-O-phenoxythiocarbonyl-6-O-trityl-β-D-glucopyranosyl)-N(4)-benzoyl cytosine (1160244-75-6)

Guidance literature:

With dmap; In acetonitrile; at 20 ℃;

DOI:10.1016/j.ejmech.2009.01.020

upstream raw materials:

1-(2-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N⁴-benzoyl cytosine

trityl chloride

Downstream raw materials:

1-(3-deoxy-3-fluoro-6-O-trityl-β-D-glycero-hex-2-enopyranosyl-4-ulose)-N⁴-benzoyl cytosine

1-(2-O-acetyl-3-deoxy-3-fluoro-4-O-phenoxythiocarbonyl-6-O-trityl-β-D-glucopyranosyl)-N(4)-benzoyl cytosine

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