Technology Process of C10H8BrN3O
There total 5 articles about C10H8BrN3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron dimethyl-trifluoro sulphide;
In
dichloromethane; 1,2-dichloro-ethane;
Reflux;
Inert atmosphere;
DOI:10.1016/j.bmcl.2011.12.015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Jones reagent / acetone / 0.5 h / 0 °C / Inert atmosphere
2: sodium carbonate / acetonitrile / 8 h / Reflux; Inert atmosphere
3: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere
With
Jones reagent; boron dimethyl-trifluoro sulphide; sodium carbonate;
In
dichloromethane; 1,2-dichloro-ethane; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2011.12.015
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate / acetonitrile / 8 h / Reflux; Inert atmosphere
2: boron dimethyl-trifluoro sulphide / dichloromethane; 1,2-dichloro-ethane / Reflux; Inert atmosphere
With
boron dimethyl-trifluoro sulphide; sodium carbonate;
In
dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.12.015