[palladium(R,R-dipamp)(η3-allyl)]ClO4

Base Information

Chemical Name:[palladium(R,R-dipamp)(η3-allyl)]ClO4
CAS No.:95070-86-3
Molecular Formula:C₃₁H₃₃O₂P₂Pd*ClO₄
Molecular Weight:705.42
Hs Code.:

Synonyms:[palladium(R,R-dipamp)(η3-allyl)]ClO4

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [palladium(R,R-dipamp)(η3-allyl)]ClO4

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Technology Process of [palladium(R,R-dipamp)(η3-allyl)]ClO4

There total 1 articles about [palladium(R,R-dipamp)(η3-allyl)]ClO4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: dichloro(η3-allyl)palladium(II)

: 55739-58-7,63449-62-7,63589-61-7,97858-62-3
(1R,2R)-1,2-bis((2-methoxyphenyl)(phenyl)phosphino)ethane

: 95070-86-3
[palladium(R,R-dipamp)(η3-allyl)]ClO4

Guidance literature:: With silver perchlorate; In dichloromethane; acetone; byproducts: silver chloride; addn. of an AgClO4/acetone soln. to a soln. of the Pd complex in CH2Cl2under argon, stirring for 30 min, filtn., addn. of the phosphine in acetone at -78°C, slow warming to 25°C; removal of the solvents under reduced pressure, dissolving the residue in methanol, addn. of water, stirring for 30 min, standing at 5°Cfor 12 h, collection of the solid, washing with ether, drying, elem. anal.;
DOI:10.1021/ja00293a038